Lead determination in glasses by laser-induced breakdown spectroscopy

Spectrochimica Acta - Part B Atomic Spectroscopy

Volumn 62, Issue 2, 2007, Pages 94-100

  Carmona, N ^a   Oujja, M ^b   Gaspard, S ^b   Garcia Heras M ^a,c   Villegas, M A ^a   Castillejo, M ^b  

^a DEPARTMENT OF PHYSICAL METALLURGY   (Spain)

^b INSTITUTO DE QUÍMICA FÍSICA ROCASOLANO   (Spain)

^c Centro de Ciencias Humanas y Sociales   (Spain)

Author keywords

Glass corrosion; Laser induced breakdown spectroscopy (LIBS); Lead glasses; Pb content; Scanning electron microscopy energy dispersive X ray analysis (SEM EDX)

Indexed keywords

CHEMICAL ATTACK; CORROSION; ENERGY DISPERSIVE X RAY ANALYSIS; LASER APPLICATIONS; SCANNING ELECTRON MICROSCOPY; SPECTROSCOPIC ANALYSIS;

CRYSTAL GLASS; GLASS CORROSION; LASER-INDUCED BREAKDOWN SPECTROSCOPY (LIBS); LEAD GLASSES; X-RAY FLUORESCENCE;

GLASS;

EID: 34047180675     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.sab.2007.01.003     Document Type: Article

References (31)

1. UNE 43-603-79, Glass. Nomenclature and terminology. Crystal Sonorous glass, 1979.
2. Fernández Navarro J.M. El Vidrio. Constitución, fabricación, propiedades. Consejo Superior de Investigaciones Científicas, Madrid (2003)
3. Moretti C. English lead crystal. The Ravenscroft recipe and points not clear on the process of development of "flint" glass formulation. Proc. of the 16th Congress of the AIHV, London, 7-13 September 2003 (2005)
4. García-Heras M., Carmona N., Gil C., and Villegas M.A. Estudio analítico de la araña de la capilla Palafox (catedral de Burgo de Osma, Soria). Proc. of the III Int. Congress AR&PA 2002, Valladolid, November 2002 (2004), Dip. Provincial de Valladolid & Junta de Castilla y León 431-440
5. García-Heras M., Carmona N., Gil C., and Villegas M.A. Neorenaissance/neobaroque stained glass windows from Madrid: a characterisation study of some panels signed by the Maumejean Fréres company. J. Cult. Herit. 6 (2005) 91-98
6. Wang P.W., and Zhang L. Structural role of lead in lead silicate glasses derived from XPS spectra. J. Non-Cryst. Solids 194 (1996) 129-134
7. 2 glasses submitted to accelerated weathering. J. Eur. Ceram. Soc. 25 (2005) 903-910
8. Hand R.J. The ballidon glass burial experiment - 35 years on. Glass Technol. 46 3 (2005) 237-242
9. Anglos D. Laser-induced breakdown spectroscopy in art and archaeology. Appl. Spectrosc. 55 (2001) 186-205
10. 2 matrix using laser-induced breakdown spectroscopy. Spectrochim. Acta Part B 56 (2001) 1419-1429
11. Bustamante M.F., Rinaldi C.A., and Ferrero J.C. Laser-induced breakdown spectroscopy characterization of Ca in soil depth profile. Spectrochim. Acta Part B 57 (2002) 303-309
12. Klein S., Stratoudaki T., Zafiropulos V., Hildenhagen J., Dickmann K., and Lehmkuhl Th. Laser-induced breakdown spectroscopy for on-line control of laser cleaning of sandstone and stained glass. Appl. Phys., A 69 (1999) 441-444
13. Melessanaki K., Mateo M., Ferrence S.C., Betancourt P.P., and Anglos D. The application of LIBS for the analysis of archaeological ceramic and metal artefacts. Appl. Surf. Sci. 197-198 (2002) 156-163
14. Oujja M., Vila A., Rebollar E., García J.F., and Castillejo M. Identification of inks and structural characterization of contemporary artistic prints by laser-induced breakdown spectroscopy. Spectrochim. Acta Part B 60 (2005) 1140-1148
15. Scholten J.H., Teule J.M., Zafiropulos V., and Heeren R.M.A. Controlled laser cleaning of painted artworks using accurate beam manipulation and on-line LIBS-detection. J. Cult. Herit. 1 (2000) 215-220
16. Castillejo M., Martín M., Silva D., Stratoudaki T., Anglos D., Burgio L., and Clark R.J.H. Analysis of pigments in polychromes by use of laser-induced breakdown spectroscopy and Raman microscopy. J. Mol. Struct. 550-551 (2000) 191-198
17. Burgio L., Corsi M., Fantoni R., Palleschi V., Sialvetta A., Squarcialuppi M.C., and Tognoni E. Self-calibrated quantitative elemental analysis by laser-induced plasma spectroscopy: application to pigments analysis. J. Cult. Herit. 1 (2000) 281-286
18. Carmona N., Oujja M., Rebollar E., Römich H., and Castillejo M. Analysis of corroded glasses by laser induced breakdown spectroscopy. Spectrochim. Acta Part B 60 (2005) 1155-1162
19. Yaroshchyk P., Body D., Morrison R.J.S., and Chadwick B.L. A semi-quantitative standard-less analysis method for laser-induced breakdown spectroscopy. Spectrochim. Acta Part B 61 (2006) 200-209
20. Colao F., Fantoni R., Lazic V., and Spizzichino V. Laser-induced breakdown spectroscopy for semiquantitative and quantitative analyses of artworks-application on multilayered ceramics and copper based alloys. Spectrochim. Acta Part B 57 (2002) 1219-1234
21. Kuzuya M., Murakami M., and Maruyama N. Quantitative analysis of ceramics by laser-induced breakdown spectroscopy. Spectrochim. Acta Part B 58 (2003) 957-965
22. Corsi M., Cristoforetti G., Hidalgo M., Legnaioli S., Palleschi V., Salvetti A., Tognoni E., and Vallebona C. Double pulse, calibration-free laser-induced breakdown spectroscopy: a new technique for in situ standard-less analysis of polluted soils. Appl. Geochem. 21 (2006) 748-755
23. Bouquillon A., and Bonnet C. Durabilité des verres au plomb dans des environments extrêmes: Apports des données archéologiques et de l'approche expérimentale. Verre 10 6 (2004) 36-41
24. Bertoncello R., Milanese L., Bouquillon A., Dran J.C., Mille B., and Salomon J. Leaching of lead silicate glasses in acid environment: compositional and structural changes. Appl. Phys., A 79 (2004) 193-198
25. Bonnet C., Bouquillon A., Turrel S., Deram V., Mille B., Salomon J., and Thomassin J.H. Alteration of lead silicate glasses due to leaching in heated acid solutions. J. Non-Cryst. Solids 323 (2003) 214-220
26. ISO 1776. Glass. Resistance to Attack by Hydrolytic Acid at 100 Degrees C. Flame Emission of Flame Atomic Absorption (1985)
27. ISO 695. Glass. Resistance to Attack by a Boiling Aqueous Solution of Mixed Alkali. Method of Test and Classification (1975)
28. Castillejo M., Martín M., Oujja M., Rebollar E., Domingo C., García-Ramos J.V., and Sánchez-Cortés S. Effect of wavelength on the laser cleaning of polychromes on wood. J. Cult. Herit. 4 (2003) 243-249
29. Siegel J., Epurescu G., Perea A., Gordillo-Vázquez F.J., Gonzalo J., and Afonso C.N. Temporally and spectrally resolved imaging of laser-induced plasmas. Optics Lett. 29 (2004) 2228-2230
30. NIST Electronic Database. Available at http://physics.nist.gov/cgi-bin/AtData/lines-form.
31. Müller K., and Sterge H. Evaluation of the analytical potential of laser-induced breakdown spectroscopy (LIBS) for the analysis of historical glasses. Archaeometry 45 (2003) 421-433