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Chemistry - A European Journal

Volumn 13, Issue 6, 2007, Pages 1724-1730

Cristallographic and chiroptical studies on tetraarylferrocenes for use as chiral rotary modules for molecular machines

(5) Muraoka, Takahiro a Kinbara, Kazushi a,b Wakamiya, Atsushi c Yamaguchi, Shigehiro c Aida, Takuzo a

a UNIVERSITY OF TOKYO (Japan)

b JAPAN SCIENCE AND TECHNOLOGY AGENCY (Japan)

c NAGOYA UNIVERSITY (Japan)

Author keywords

Absolute configuration; Chirality; Circular dichroism; Metallocenes; Molecular devices

Indexed keywords

AROMATIC COMPOUNDS; CHIRALITY; CORRELATION METHODS; CRYSTAL STRUCTURE; DICHROISM;

ABSOLUTE CONFIGURATION; MOLECULAR DEVICES;

ORGANOMETALLICS;

EID: 33947692359 PISSN: 09476539 EISSN: 15213765 Source Type: Journal
DOI: 10.1002/chem.200601098 Document Type: Article

Times cited : (24)

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- To represent the chiroptical features of chiral compounds, the sign of the CD band at λ = 260nm is utilized because this band is commonly observed for all the compounds that contain a chiral ferrocene unit.

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- Crystal data and structural refinement parameters: trans-1(CHCI 3)0.5, C50.5)H40.5)CI 1.5)FeN2)i; MI, 784.42; monoclinic; space group P21),/c; a, 20.092(12, b, 5.907(3, c, 33.09(2)Å; α, γ, 90, β= 96.052(2)°; K, 3906(4)å3; Z, 4; R, 0.0714; wR, 0.0755 (for 11970 data and 555 refined parameters, ) CD260-(1S.l'S)-10-acetone: C73)H 70)FeN2)O7)S2, M 3)=1207.33; monoclinic; space group C2; a, 32.997(6, b= 8.4674(13, c, 24.442(4) Å; α =γ, 90, ß= 113.0452(7)°; V, 6284.1(18) Å131; Z, 4, R, 0.0587; wR, 0.0668 (for 13056 data and 839 refined parameters, CCDC-611823 (trans-1(CHC3) 0.5) and -611824, )CD260(1S.l'S)-10- acetone) contain the supplementary crystallog
- 260(1S.l'S)-10- acetone) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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