Restricted Rotation Involving the Tetrahedral Carbon. V. Direct Observation of the Hindered Rotation of a Methyl Group by High Resolution Nuclear Magnetic Resonance Spectroscopy1

Journal of the American Chemical Society

Volumn 95, Issue 21, 1973, Pages 7169-7171

  Nakamura, Mikio ^a   Ōki, Michinori ^a   Nakanishi, Hiroshi ^b  

^a UNIVERSITY OF TOKYO   (Japan)

^b Natl Chem Laboratory for Industry   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33947087034     PISSN: 00027863     EISSN: 15205126     Source Type: Journal    
DOI: 10.1021/ja00802a052     Document Type: Letter

References (15)

1. H. Nakanishi, O. Yamamoto, M. Nakamura, and M. Oki, Tetrahedron Lett., 727 (1973).
2. J. R. During, et al., J. Chem. Phys., 52, 2046 (1970).
3. Allinger, et al., J. Amer. Chem. Soc., 90, 1199 (1968).
4. E. O. Stejskal, D. E. Woessner, T. C. Farrar, and H. S. Gutowsky, J. Chem. Phys., 31, 55 (1959).
5. G. W. Smith, J. Chem. Phys., 42, 4229 (1965).
6. E. R. Andrew and P. C. Canepa, J. Magn. Resonance, 7, 429 (1972).
7. P. S. Allen and A. Cowking, J. Chem. Phys., 47, 4286 (1967).
8. P. S. Allen and A. Cowking, J. Chem. Phys., 49, 789 (1968).
9. A. Saika, A. Kawamori, and R. Takagi, J. Magn. Resonance, 7, 324 (1972).
10. K. D. Bartle, P. M. G. Bavin, D. W. Jones, and R. L'Amie, Tetrahedron, 26, 911 (1970).
11. J. P. N. Brewer, H. Heaney, and B. A. Marples, Chem. Commun., 27 (1967).
12. M. Oki and M. Suda, Bull. Chem. Soc. Jap., 44, 1876 (1971).
13. M. Oki and G. Yamamoto, Chemistry Lett., 45 (1972).
14. N. M. Sergeyev, K. F. Abdulla, and V. R. Skvarchenko, J. Chem, Soc., Chem. Commun., 368 (1972).
15. H. Heaney and J. M. Jablonski, J. Chem. Soc. C, 1895 (1968).