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Volumn , Issue 3, 2007, Pages 395-398

Octanol-accelerated Baylis-Hillman reaction

Author keywords

Additive; Aliphatic aldehydes; Baylis Hillman reaction; Octanol; Rate acceleration

Indexed keywords

ALDEHYDE; CYCLOHEXANOL; METHANOL; OCTANOL;

EID: 33847414560     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2007-968032     Document Type: Article
Times cited : (27)

References (34)
  • 20
    • 0000892247 scopus 로고    scopus 로고
    • Paquette, L. A, Ed, Wiley: New York
    • (c) Ciganek, E. In Organic Reactions, Vol. 51; Paquette, L. A., Ed.; Wiley: New York, 1997, 201.
    • (1997) Organic Reactions , vol.51 , pp. 201
    • Ciganek, E.1
  • 30
    • 0029889688 scopus 로고    scopus 로고
    • Schuurman, R. J. W.; v. d. Linden, A.; Grimbergen, R. P. F.; Nolte, R. J. M.; Scheeren, H. W. Tetrahedron 1996, 52, 8307.
    • (c) Schuurman, R. J. W.; v. d. Linden, A.; Grimbergen, R. P. F.; Nolte, R. J. M.; Scheeren, H. W. Tetrahedron 1996, 52, 8307.
  • 33
    • 33847380066 scopus 로고    scopus 로고
    • Spectroscopic Data for Compound 4. IR(neat, 3415, 1665, 1635, 1088 cm-1. 1H NMR (400 MHz, CDCl3, δ, 1.32 (d, J, 6.5 Hz, 3 H, 2.36 (s, 3 H, 3.31 (br s, 1 H, 4.66 (br s, 1 H, 6.08 (s, 1 H, 6.11 (s, 1 H, 13C NMR (100 MHz, CDCl 3, δ, 200.19, 151.09, 124.27, 65.89, 25.90, 21.76. HRMS (ESI, m/z calcd for C6H10O2 [M, H, 114.0681; found: 114.0685. Spectroscopic Data for Compound 6. 1H NMR (400 MHz, CDCl3, δ, 6.04 (s, 1 H, 5.85 (s, 1 H, 2.61-2.57 (m, 1 H, 2.55-2.50 (m, 1 H, 2.34 (s, 3 H, 2.13 (s, 3 H, 13C NMR 100 MHz, CDCl3, δ, 207.59, 199.24, 147.52, 126.01, 42.20, 29.47, 25.61, 25.05
    • 3): δ = 207.59, 199.24, 147.52, 126.01, 42.20, 29.47, 25.61, 25.05.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.