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33847371348
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Structural data of 2: monoclinic, space group P2/c, a, 2053.9(1, b, 1011.4(1, c, 1889.8(1) pm; β= 105.21(1)°, V, 3788.2(5)·106 pm3, Z, 4, ρcal, 2.053 gcm-3. Crystal size: 0.31×0.16×0.04 mm. Data collection for C37H30I5P2: IPDSI (Stoe, Mo-Kα, T, 193 K, 36580 collected, 7322 independent, 5149 observed (F0>4σ(F0) reflections, 399 parameters, absorption correction: numerical. Structure solution and refinement: SHELXS-97, SHELXL-97 [23, R1, 0.0261, wR2, 0.0517. More details have been deposited with the Cambridge Crystallographic Centre under the deposition number CCDC-623120
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2 = 0.0517. More details have been deposited with the Cambridge Crystallographic Centre under the deposition number CCDC-623120.
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21
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