Synthesis and characterization of nickel phosphonopropionate hybrid materials

Inorganic Chemistry Communications

Volumn 10, Issue 4, 2007, Pages 447-450

  Chen, Zhenxia ^a   Weng, Linhong ^a   Zhao, Dongyuan ^a  

^a FUDAN UNIVERSITY   (China)

Author keywords

4,4 Bipyridine; Crystal structure; Hydrothermal synthesis; Nickel phosphonates

Indexed keywords

EID: 33847335897     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2007.01.002     Document Type: Article

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20. 2O (10 ml, 555.6 mmol) was heated at 70 °C for 2 days. Product II was obtained in 76.3% yield based on 4,4′-bipyridine. XRD patterns are consistent with simulated single-crystal patterns [20], revealing that both products are pure phase materials. Elemental analysis [21] for compound I, Calcd. N, 9.075%; C, 46.69%; H, 4.136%, Found: N, 9.058%; C, 46.44%; H, 4.076%. For compound II, Calcd. N, 6.381%; C, 35.57%; H, 4.823%. Found: N, 6.408%; C, 35.63%; H, 4.844%.
21. 2 is 1.037.
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23. -1.
24. -1, from 30 to 900 °C.
25. Variable-temperature magnetic susceptibility measurements were carried out in the 2-300 K range using a Quantum Design PPMS-9T magnetometer at a magnetic field of 10,000 Oe.
26. Powder XRD data were obtained from a Bruker D4 diffractometer with Cu Kα radiation (λ = 1.5418 Å).
27. Elemental analyses were carried out on an Elementar Vario EL III microanalyzer.
28. Sheldrick G.M. SHELXS 97, Program for X-ray Crystal Structure Solution and Refinement (1997), University of Gottingen, Germany