Densitometric determination of fenbendazole in veterinarian suspension: Validation of the method

Journal of Liquid Chromatography and Related Technologies

Volumn 30, Issue 4, 2007, Pages 489-498

  Cholifah, Siti ^a   Noviansari, Anna ^a   Kartinasari, Wiwin Farina ^a   Indrayanto, Gunawan ^b  

^a Bernofarm Pharmaceutical Company   (Indonesia)

^b AIRLANGGA UNIVERSITY   (Indonesia)

Author keywords

Densitometry; Fenbendazole; Syrup Suspension; TLC; Validation

Indexed keywords

DENSITY MEASUREMENT (SPECIFIC GRAVITY); DRUG PRODUCTS; ENERGY ABSORPTION; QUALITY CONTROL; REFLECTION; SILICA GEL; VETERINARY MEDICINE;

FENBENDAZOLE; PRECOATED SILICA GEL TLC PLATES; TLC DENSITOMETRIC METHOD; VETERINARIAN SUSPENSION;

ALCOHOLS;

ACETIC ACID ETHYL ESTER; DICHLOROMETHANE; FENBENDAZOLE; FORMIC ACID; HYDROCHLORIC ACID; METHANOL; SILICA GEL; VETERINARY DRUG;

ARTICLE; DENSITOMETRY; DRUG INDUSTRY; MEDICAL EXAMINATION; QUALITY CONTROL; QUANTITATIVE ANALYSIS; REFLECTOMETRY; SOLUTION AND SOLUBILITY; SUSPENSION; THIN LAYER CHROMATOGRAPHY; VALIDATION PROCESS;

EID: 33847151790     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070601093788     Document Type: Article

References (24)

1. Environmental Assessment, NADA 128-620 (www.fda.gov/cvm/FO/128-620EA.pdf; accessed on June 27, 2006).
2. The United States Pharmacopoeia 28-National Formulary 23, First Supplement; United States Pharmacopoeial Convention: Rockville, MD, 2004, 3326-3327.
3. European Pharmacopoeia, 5th Ed.; Council of Europe: Strasbourg, Cedex, 2004, 1577-1578.
4. Mottier, L.; Alvarez, L.; Lanusse, C. Quantitative chromatographic determination of several anthelmintic molecules in parasite material. J. Chromatogr. B 2003, 798, 117-125.
5. Szprengier-Juszkiewicz, T.; Semeniuk, S.; Wlodarczyk, B. Plasma kinetic and tissue residue of fenbendazole following oral administration to pigs. Bull. Vet. Inst. Pulawy 2002, 46, 119-125.
6. Blanchflower, W.J.; Cannavan, A.; Kennedy, D.G. Determination of fenbendazole and oxfendazole in liver and muscle using liquid chromatography-mass spectrometry. Analyst 1994, 119, 1325-1328.
7. Sorensen, L.K.; Hansen, H. Determination of fenbendazole and its metabolite by a high-performance liquid chromatography method. Analyst 1998, 123, 2559-2562.
8. Barker, S.A.; Hsieh, L.C.; Short, C.R. Methodology for the analysis of fenbendazole ant its metabolite in plasma, urine, feces, and tissue homogenates. Anal. Biochem. 1986, 155, 112-118.
9. Msagati, T.M.; Nindi, M.M. Determination of benzimidazole anthelmintic compounds by supported liquid membrane extraction and liquid chromatography. J. Sep. Sci. 24, 606-614.
10. Fletouris, D.; Botsoglou, N.; Psomas, I.; Mantis, A. Rapid quantitative screening assay of benzimidazole in milk by liquid chromatography. J. AOAC Int. 1996, 79, 1281-1287.
11. Barker, S.A.; Hsieh, L.C.; McDowell, T.R.; Short, C.R. Qualitative and quantitative analysis of anthelmintic fenbendazole and its metabolites in biological matrices by direct exposure probe mass spectrometry. Biomed. Environ. Mass. Spectrom. 1987, 14, 161-165.
12. Rayput, S.J.; Prabhakar, A.; Sadhana, J.; Prabhakar, A.K. Spectrophotometric method for fenbendazole. Indian J. Pharm. Sci. 1996, 58, 132-133.
13. Sastry, C.S.P.; Sama, V.A.N.; Prasad, U.V.; Lakshmi, C.S.R. N-Bromosuccinimide as an analytical reagent for the spectrophotometeric determination of benzimidazole anthelmintics. Indian. J. Pharm. Sci. 1997, 59, 161-164.
14. Brandon, D.L.; Bates, A.H.; Binder, R.G.; Montague, W.C. Food and Agriculture Immunology 2002, 14, 275-283.
15. de Olivera, M.F.; Stradiotto, N.R. Voltametric determination in veterinarian formulation. J. Pharm. Biomed. Anal. 2002, 30, 279-284.
16. Botsoglou, N.A.; Fletouris, D.J.; Psomas, I.E. Rapid extraction and ion-pair liquid chromatographic determination of fenbendazole in poultry feeds. J. Liq. Chromatogr. & Rel. Technol. 2000, 23, 433-444.
17. Gomes, A.R.; Nagaraju, V. High-performance liquid chromatographic separation and determination of the process related impurities of mebendazole, fenbendazole and albendazole in bulk drugs. J. Pharm. Biomed. Anal. 2001, 26, 919-927.
18. CBS, CD room Version, 51-96, Camag, Muttenz, 2005.
19. Funk, W.; Damman, V.; Donnervert, G. Qualitätssicherung in der Analytischen Chemie; VCH: Weinheim, New York, Basel, Cambridge, 1992, Vol. 12-36; 161-180.
20. Ferenczi-Fodor, K.; Vegh, Z.; Nagy-Turak, A.; Renger, B.; Zeller, M.J. Validation and quality assurance of planar chromatography procedures in pharmaceutical analysis. AOAC Inter. 2001, 84, 1265-1276.
21. Yuwono, M.; Indrayanto, G. Validation method of analysis by using Chromatography. In Profiles of Drugs Substances, Excipients and Related Methodology; Brittain, H., Ed.; Elsevier Academic Press: San Diego, New York, Boston, London, Sydney, Tokyo, Toronto, 2005, Vol. 32; 243-258.
22. Carr, G.P.; Wahlich, J.C. A practical approach to method validation in pharmaceutical analysis. J. Pharm. Biomed. Anal. 1990, 8, 613-618.
23. Kromidas, S. Validierung in der Analytik; Wiley-VCH: Weinheim, New York, Chichester, Brisbane, Singapore, Toronto, 1999, 56-85, 110-113.
24. Ermer, J. Validation in pharmaceutical analysis, Part I: An integrated approach. J. Pharm. Biomed. Anal. 2001, 24, 755-767.