Single-crystal growth and characterization of disilver(I) monofluorophosphate(V), Ag2PO3F: Crystal structure, thermal behavior, vibrational spectroscopy, and solid-state 19F, 31P, and 109Ag MAS NMR spectroscopy

Inorganic Chemistry

Volumn 46, Issue 3, 2007, Pages 801-808

  Weil, Matthias ^a   Puchberger, Michael ^b   Füglein, Ekkehard ^c   Baran, Enrique J ^d   Vannahme, Julia ^e   Jakobsen, Hans J ^f   Skibsted, Joørgen ^f  

^a VIENNA UNIVERSITY OF TECHNOLOGY   (Austria)

^b VIENNA UNIVERSITY OF TECHNOLOGY   (Austria)

^c NETZSCH GERÄTEBAU GMBH   (Germany)

^d FACULTAD DE CIENCIAS EXACTAS   (Argentina)

^e UNIVERSITY OF MÜNSTER   (Germany)

^f AARHUS UNIVERSITY   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

FLUORIDE; FLUOROPHOSPHATE; ISOTOPE; PHOSPHATE; PHOSPHORUS; SILVER;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; CRYSTALLIZATION; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHASE TRANSITION; TEMPERATURE;

CRYSTALLIZATION; FLUORIDES; ISOTOPES; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR STRUCTURE; PHASE TRANSITION; PHOSPHATES; PHOSPHORUS ISOTOPES; SILVER; SPECTROSCOPY, FOURIER TRANSFORM INFRARED; TEMPERATURE;

EID: 33847148006     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic061765w     Document Type: Article

References (69)

1. II is an alkaline earth metal, a first row transition metal, or tin; the water content x can range from 0 to 5.
2. Ericsson, S. Y. U.S. Patent 3,119,743, Jan. 28, 1964.
3. Möwius, F.; Meisel, M.; Grunze, H.; Kolditz, L.; Zelbig, M.; Öse, W.; Standfuss, D.; Kirk, H.; Hesse, R.; Götze, H.; Unger, W. U.S. Patent 4,767,458, Aug. 30, 1998.
4. (a) Duprat, M.; Lafont, M. C.; Moran, F.; Rocher, S. Rev. Fr. Sci. Eau 1985, 4, 1-15.
5. (b) Durand, J.; Larbot, A.; Cot, L.; Duprat, M.; Dabosi, F. Z. Anorg. Allg. Chem. 1983, 504, 163-72.
6. (c) Laamari, M. R.; Derja, A.; Benzakour, J.; Berraho, M. Ann. Chim. 2001, 26, 117-130.
7. (d) Laamari, M. R.; Derja, A.; Benzakour, J.; Berraho, M. J. Electroanal. Chem. 2004, 569, 1-6.
8. (e) Chaussadent, T.; Nobel-Pujol, V.; Farcas, F.; Mabille, I.; Fiaud, C. Cem. Concr. Res. 2006, 36, 556-561.
9. Boffardi, B. P.; Sherbondy, A. M. European Patent (EP) 481,669, April 22, 1992.
10. (a) Lioté, F.; Bardin, C.; Liou, A.; Brouard, A.; Terrier, J.-L.; Kuntz, D. Calcif. Tissue Int. 1992, 50, 209-13.
11. (b) Ringe, J. D.; Kipshoven, C.; Coster, A.; Umbach, R. Osteoporosis Int. 1999, 9, 171-178.
12. (c) Duff, E. J. Caries Res. 1983, 17 (Suppl 1), 77-87.
13. (d) Root, M. J.; Schreiber, R. S. Caries Res. 1990, 24, 30-2.
14. (e) Bruun, C.; Givskov, H. Caries Res. 1993, 27, 96-99.
15. (f) Billington, R. W.; Williams, J. A.; Dorban, A.; Pearson, G. J. Biomaterials 2004, 25, 3399-3402.
16. Lange, W. Ber. Dtsch. Chem. Ges. 1929, 62B, 793-801.
17. Schülke, U.; Kayser, R. Z. Anorg. Allg. Chem. 1991, 600, 221-226.
18. Sheldrick, G. M. SADABS; University of Göttingen: Göttingen, Germany.
19. Sheldrick, G. M. SHELXTL, version 6.14; Bruker AXS Inc.; Madison, WI.
20. Gelato, L. M.; Parthé, E. J. Appl. Crystallogr. 1987, 20, 139-143.
21. Brown, I. D. The Chemical Bond in Inorganic Chemistry; Oxford University Press: Oxford, U.K., 2002.
22. Brese, N. E.; O'Keeffe, M. Acta Crystallogr. 1991, B47, 192-197.
23. Dowty, E. ATOMS for Windows, version 6.2; Shape Software: Kingsport, TN, 2001.
24. Baran, E. J.; Aymonino, P. J. Spectrochim. Acta 1968, 24A, 288-291.
25. Jakobsen, H. J.; Daugaard, P.; Hald, E.; Rice, D.; Kupce, E.; Ellis, P. D. J. Magn. Reson. 2002, 156, 152-154.
26. Skibsted, J.; Nielsen, N. C.; Bildsøe, H.; Jakobsen, H. J. J. Magn. Reson. 1991, 95, 88-117;
27. Chem. Phys. Lett. 1992, 188, 405-412.
28. Müller-Buschbaum, Hk. Z. Anorg. Allg. Chem. 2004, 630, 2125-2175.
29. Weil, M. Z. Naturforsch. 2003, 58b, 1091-1096.
30. Corbridge, D. E. C. The Structural Chemistry of Phosphorus; Elsevier: Amsterdam, 1974.
31. Weil, M.; Puchberger, M.; Baran, E. J. Inorg. Chem. 2004, 43, 8330-8335.
32. Payen, J.; Durand, J.; le Cot, L.; Galigne, J. L. Can. J. Chem. 1979, 57, 886-889.
33. Durand, J.; le Cot, L.; Galigne, J. L. Acta Crystallogr. 1974, B30, 1565-1569.
34. Berndt, A. F. Acta Crystallogr. 1974, B30, 529-530.
35. 25f (a) Prescott, H. A.; Troyanov, S. I.; Kemnitz, E. J. Solid State Chem. 2001, 156, 415-421.
36. (b) Levy, A. H.; Lisensky, G. C. Acta Crystallogr. 1978, B34, 3502-3510.
37. (c) Payen, J. L.; Durand, J.; Cot, L.; Galigné, J.-L. Can. J. Chem. 1979, 57, 886-889.
38. (d) McGinnety, J. A. Acta Crystallogr. 1972, B28, 2845-2852.
39. (e) Bengtsson, E. Arkiv Kemi. Mineral. Geol. 1941, 15b, 8.
40. (f) Hill, R. J. Can. Mineral. 1977, 15, 522-526.
41. Mehrotra, B. N.; Hahn, T.; Eysel, W.; Roepke, H.; Illguth, A. Neues Jahrb. Mineral., Monatsh. 1978, 408-421.
42. Ross, S. D. Inorganic Infrared and Raman Spectra; McGraw Hill: London, 1972.
43. Müller, A.; Baran, E. J.; Carter, R. O. Struct. Bonding 1976, 26, 81-139.
44. Fadini, A.; Schnepel, F. M. Vibrational Spectroscopy: Methods and Applications; Ellis Horwood: Chichester, U.K., 1989.
45. Siebert, H. Anwendungen der Schwingungsspektroskopie in der Anorganischen Chemie; Springer-Verlag: Berlin, 1966.
46. Müller, A. Z. Naturforsch. 1966, 21a, 433-436.
47. Baran E. J.; Ferrer E. G.; Bueno I.; Parada C.; J. Raman Spectrosc. 1990, 21, 27-30.
48. Yamada, T; Koizumi, H; J. Cryst. Growth 1983, 64, 558-562.
49. CRC Handbook of Chemistry and Physics, 76th ed., CRC Press: Boca Raton, FL, 1995.
50. Allaf, A. W. Spectrochim. Acta 1998, A54, 921-926.
51. http://webbook.nist.gov/chemistry.
52. (a) Heide, K.; Menz, D. H.; Schmidt, C.; Kolditz, L. Z. Anorg. Allg. Chem. 1985, 520, 32-38.
53. (b) Menz, D. H.; Heide, K.; Kunert, C.; Mensing, C.; Kolditz, L. Z. Anorg. Allg. Chem. 1986, 540, 191-197.
54. (c) Möwius, F.; Ziemer, B.; Reck, G.; Meisel, M.; Grunze, H. Z. Anorg. Allg. Chem. 1987, 547, 75-82.
55. (d) Jäger, C.; Ehrt, D.; Haubenreisser, U. Z. Phys. Chem. 1988, 159, 75-87.
56. Turner, G. L.; Smith, K. A.; Kirkpatrick, R. J.; Oldfield, E. J. Magn. Reson. 1986, 70, 408-415.
57. (a) Duncan, T. M.; Douglass, D. C. Chem. Phys. 1984, 87, 339-349.
58. (b) Hartmann, P.; Vogel, J.; Schnabel, B. J. Magn. Reson., Ser. A 1994, 111, 110-114.
59. (c) Fyfe, C. A.; Meyer zu Altenschildesche, H.; Skibsted, J. Inorg. Chem. 1999, 38, 84-92.
60. Haubenreisser, U.; Sternberg, U.; Grimmer, A.-R. Mol. Phys. 1987, 60, 151-163.
61. (a) VanderHart, D. L.; Gutowsky, H. S.; Farrar, T. C. J. Chem. Phys. 1969, 50, 1058-1065.
62. (b) Grimmer, A. R.; Müller, D.; Neels, J. Z. Chem. 1983, 23, 140-142.
63. (c) Grimmer, A. R.; Jost, K. H.; Müller, D.; Neels, J. J. Fluorine Chem. 1987, 34, 347-360.
64. (d) Farrar, T. C.; Jablonsky, M. J. J. Phys. Chem. 1991, 95, 9159-9166.
65. (e) Farrar, T. C.; Trudeau, J. D. NATO Sci. Ser., Ser. C 1993, 386, 27-48.
66. (f) Farrar, T. C.; Schwartz, J. L.; Rodríguez, S. J. Phys. Chem. 1993, 97, 7201-7207.
67. (g) Prescott, H. A.; Troyanov, S. I.; Kemnitz, E. Z. Kristallogr. 2000, 215, 240-245.
68. van Wuellen, L.; Vensky, S.; Hoffbauer, W.; Jansen, M. Solid State Sci. 2005, 7, 920-924.
69. Penner, G. H.; Li, W. Inorg. Chem. 2004, 43, 5588-5597.