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X-ray data for compound 2a: C20H17IO 4, MW, 448.24, T, 298-(2) K, λ, 0.71073 Å, monoclinic space group, P-1, a, 7.615(16) Å, b, 9.91(2) Å, c, 12.33(2) Å, α, 98.11(2)°, β= 96.80(2)°, γ, 96.61(3)°, V, 906(3) Å3, Z, 2, D c, 1.642 mg/m3, μ, 1.787 mm-1, F(000, 444, crystal size 0.50 × 0.45 × 0.38 mm3, independent reflections 3045 [R (int, 0.0485, reflections collected 4244, refinement method, full-matrix least-squares on F2, goodness-of-fit on F2 1.008, final R indices [I > 2σ-(1, R1, 0.0789, wR2, 0.1902. R indices (all date) R1, 0.0992, wR2, 0.2136, largest diff. peak and hole 1.840 and -2.845 e Å-3 (12) For reviews, see: (a) Campbell
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