Development of a specimen heating holder with an evaporator and gas injector and its application for catalyst

Journal of Electron Microscopy

Volumn 55, Issue 5, 2006, Pages 245-252

  Takeo, Kamino ^a   Toshie, Yaguchi ^a   Mitsuru, Konno ^a   Akira, Watabe ^a   Yasuhira, Nagakubo ^b  

^a HITACHI HIGH TECHNOLOGIES CORPORATION   (Japan)

^b HITACHI LTD   (Japan)

Author keywords

Al2O3; AuPd; In situ TEM observation; Specimen heating holder

Indexed keywords

ALUMINA; ALUMINUM OXIDE; ANTENNAS; DEPOSITION; NANOPARTICLES; SYNTHESIS (CHEMICAL); TRANSMISSION ELECTRON MICROSCOPY;

CATALYST NANO PARTICLES; GAS INJECTORS; IN SITU TRANSMISSION ELECTRON MICROSCOPE OBSERVATION; IN-SITU TRANSMISSION; ITS APPLICATIONS; NANOPARTI-CLES; SPECIMEN HEATING; SPECIMEN HEATING HOLDER; TRANSMISSION ELECTRON; ]+ CATALYST;

BINARY ALLOYS;

EID: 33846966625     PISSN: 00220744     EISSN: 14779986     Source Type: Journal    
DOI: 10.1093/jmicro/dfl032     Document Type: Article

References (12)

1. Hashimoto H (1958) A specimen treating device at high temperature for the electron microscope. J. Electron Microsc. 6: 8-11.
2. Hashimoto H (1960) Crystal growth of oxide and sulphide. J. Electron Microsc. 9: 130-137.
3. Butler E P, and Hale K F (1981) Dynamic Experiments in the Electron Microscope 9 (North Hollad, New York).
4. Mori H, Komatsu K, and Fujita H (1993) Topics in in situ experiments in the HVEM. Ultramicroscopy 51: 31-40.
5. Komatsu K, and Mori H (2005) In situ HVEM study on copper oxidation using an improved environmental cell. J. Electron Microsc. 54: 99-107.
6. Sharma R, Weiss K, Mckelvey K M, and Glausinger (1994) Controlled atmosphere electron microscopy development. Proc. of the 52nd Annual Meeting of Microsc. Soc. Am. pp. 494-495.
7. Boyes E D, and Gai P L (1997) Environmental high resolution electron microscopy and application to chemical science. Ultramicroscopy 67: 219-232.
8. Kamino T, and Saka H (1993) Newly developed high resolution hot stage and its application to material science. Microsc. Microanal. Microstruct. 4: 127-135.
9. Kamino T, Yaguchi T, Konno M, Watabe A, Marukawa T, Mima T, Kuroda K, Saka H, Arai S, Makino H, Suzuki Y, and Kishita K (2005) Development of a gas injection/specimen heating holder for use with transmission electron microscope. J. Electron Microsc. 54: 497-503.
10. Kamino T, Yaguchi T, Konno M, and Hashimoto T (2005) In situ high temperature TEM observation of interactioin between multi-walled carbon nanotube and in situ deposited gold nano-particles. J. Electron Microsc. 54: 461-465.
11. Lee J-G, and Mori H (2004) Solid/liquid two-phase structures in isolated nanometer-sized alloy particles. Phys. Rev. B70: 144105-1-5.
12. Carim A H, Rohger G S, Dan Donr, Tzeng S-Y, Rohrer C L, and Perrotta A J (1997) Conversion of diaspore to corundum: a new a-Alumina transformation sequence. J. Am. Ceram. Soc., 80: 2677-2680.