Rapid identification of C21 steroidal saponins in Cynanchum versicolor Bunge by electrospray ionization multi-stage tandem mass spectrometry and liquid chromatography/tandem mass spectrometry

Rapid Communications in Mass Spectrometry

Volumn 21, Issue 3, 2007, Pages 279-285

  Zheng, Zhaoguang ^a,b   Zhang, Weidong ^a,c   Kong, Lingyi ^b   Liang, Mingjin ^a   Li, Huiliang ^a   Lin, Min ^a   Liu, Runhui ^a   Zhang, Chuan ^a  

^a SECOND MILITARY MEDICAL UNIVERSITY   (China)

^b CHINA PHARMACEUTICAL UNIVERSITY   (China)

^c SHANGHAI JIAO TONG UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

ELECTRODEPOSITION; FORMIC ACID; GLUCOSE; IONS; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLITES;

LC-ESI-MS; LC/ESI-MS; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY; MULTI-STAGES; RAPID IDENTIFICATION; SPECTRA'S; STEROIDAL SAPONINS; TANDEM MASS SPECTROMETRY; TANDEM-MASS SPECTROMETRY;

ELECTROSPRAY IONIZATION;

SAPONIN; STEROID;

ARTICLE; CHEMISTRY; CYNANCHUM; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METABOLISM; METHODOLOGY; PLANT ROOT; TIME;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CYNANCHUM; PLANT ROOTS; SAPONINS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STEROIDS; TIME FACTORS;

EID: 33846819032     PISSN: 09514198     EISSN: 10970231     Source Type: Journal    
DOI: 10.1002/rcm.2829     Document Type: Article

References (27)

1. Committee for the Pharmacopoeia of PRC. Pharmacopoeia of People's Republic of China, vol 1 Chemical Industry Press: Beijing, 2005; 273-274.
2. Bai H, Li W, Koike K, et al. Tetrahedron 2005; 61: 5797.
3. Nakagawa T, Hayashi K, Wada K, Mitsuhashi H. Tetrahedron 1983; 39: 607.
4. Zhang RS, Ye YP, Shen YM, et al. Tetrahedron 2000; 56: 3875.
5. Mellado GG, Zubia E, Ortega MJ, et al. Steroids 2004; 69: 291.
6. Halaweish FT, Huntimer E, Khalil AT. Phytochem. Anal. 2004; 15: 189.
7. Yin J, Kouda K, Tezuka Y, et al. J. Nat. Prod. 2003; 66: 646.
8. Liu HW, Xiong Z, Li F, et al. Chem. Pharm. Bull. 2003; 51: 1089.
9. Oleszek W, Bialy Z. J Chromatogr. A 2006; 1112: 78.
10. Song FJ. Chin. Tradit. Pat. Med. 2003; 25: 232.
11. Madl T, Sterk H, Mittelbach M, et al. J. Am. Soc. Mass Spectrom. 2006; 17: 795.
12. Fang SP, Hao CY, Sun WX, et al. Rapid Commun. Mass Spectrom. 1998; 12: 589.
13. Van SD , Zomer G, Van WG, Wiertz EH, et al. Phytochem. Anal. 2000; 11: 190.
14. Cui M, Song FR, Liu ZQ, et al. Rapid Commun. Mass Spectrom. 2001; 15: 586.
15. Liu YZ, Liang F, Cui LJ, et al. Rapid Commun. Mass Spectrum. 2004; 18: 235.
16. Liu SY, Cui M, Liu ZQ, et al. J. Am. Soc. Mass Spectrom. 2004; 15: 133.
17. Broberg S, Nord LI, Kenne L. J. Mass Spectrom. 2004; 39: 691.
18. Combarieu ED, Falzoni M, Fuzzati N, et al. Fitoterapia 2002; 73: 583.
19. Wolfender JL, Hostettmann K, Abe F, et al. J. Chromatogr. A 1995; 712: 155.
20. Qiu SX, Zhang ZX, Zhou J. Acta Pharm. Sinica 1990; 25: 473.
21. Qiu SX, Zhang ZX, Zhou J. Phytochemistry 1989; 28: 3175.
22. Qiu SX, Zhang ZX, Yong L, et al. Planta Med. 1991; 57: 454.
23. Nakagawa T, Hayashi K, Wada K, et al. Tetrahedron 1983; 39: 607.
24. Bai H, Li W, Koike K, et al. Tetrahedron 2005; 61: 5797.
25. Zheng ZG, Liu RH, Kong LY, et al. Chin. Chem. Lett. 2006; 17: 919.
26. Cheng DY. Analytical Chemistry. Shanghai Science and Technology Press: Shanghai, 1995; 296-297.
27. Annick P, Gabriele B, Karl H, et al. Phytochemistry 2001; 57: 489.