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Volumn 46, Issue 2, 2007, Pages 346-347

Intercalation of lodic acid into the layered uranyl iodate, UO 2(IO3)2(H2O)

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EID: 33846577795 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic062072i Document Type: Article

Times cited : (29)

References (21)

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- UO2(IO3)2(H2O) ·2HIO3 was prepared by loading UO2(NO 3)2·6H2O (0.056 g, 0.112 mmol, HIO 3 (0.585 g, 3.321mmol, and 0.5 mL of distilled and Millipore-filtered water in a 23-mL poly(tetrafluoroethylene)-lined autoclave. The autoclave was heated at 200°C for 3 days and then cooled at a rate of 9°C/h to room temperature. Clusters of yellow block crystals of UO 2(IO3)2(H2O)·2HIO 3 were isolated, washed with methanol, and allowed to dry. Yield: 59 mg 53% yield based on U, EDX analysis provided a U/I ratio of 1:4 mmol
- 3 were isolated, washed with methanol, and allowed to dry. Yield: 59 mg (53% yield based on U). EDX analysis provided a U/I ratio of 1:4 mmol.

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- 2 was by full-matrix least squares, 92 parameters.

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