SCOPUS 정보 검색 플랫폼

Volumn , Issue 2, 2007, Pages 235-238

Formation of a dative bond between Pt0 and MoII in linear Pt0-MoII-MoII-Pt0 complexes, MoII2Pt02(pyphos) 4(PR3)2, and unique 1,4-oxidative addition reaction of diaryl disulfides giving MoII2Pt I2(pyphos)

(6) Mashima, Kazushi a Shimoyama, Yuuji a Kusumi, Yoshitaka a Fukumoto, Atsushi a Yamagata, Tsuneaki a Ohashi, Masato a

a OSAKA UNIVERSITY (Japan)

Author keywords

Dative bonds; Linear clusters; Molybdenum; Oxidative addition; Platinum; Thiolates

Indexed keywords

ADDITION REACTIONS; BINARY ALLOYS; MOLYBDENUM; PLATINUM; PLATINUM ALLOYS; PLATINUM COMPOUNDS; SULFUR COMPOUNDS; X RAY CRYSTALLOGRAPHY;

CRYSTALLOGRAPHIC STUDIES; DATIVE BONDS; DITHIOLATES; LINEAR CLUSTER; OXIDATIVE ADDITION PRODUCTS; OXIDATIVE ADDITION REACTION; OXIDATIVE ADDITIONS; THIOLATES;

SPECTROSCOPIC ANALYSIS;

EID: 33846488503 PISSN: 14341948 EISSN: 10990682 Source Type: Journal
DOI: 10.1002/ejic.200601018 Document Type: Article

Times cited : (23)

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- Crystal data for 4e·1.5hexane: Fw, 2072.48 (0.27 X 0.20 X 0.10 mm, space group P1, 2, a, 14.35524(17, b, 16.24695(7, c, 19.5725(3) Å, α, 108.9657(8, β, 97.8677(6, γ, 106.1829(6)°, V, 4013.86(8) Å3, Z, 2, calculated density, 1.715 Mg/m3. Data were collected with Rigaku RAXIS RAPID imaging plate area detector with graphite monochromated Mo-Kα radiation at a temperature of 100(2) K to a maximum 2θ value of 63.0°. A total of 240 oscillation images were collected. Of the 99273 reflections that were collected, 26544 were unique Rint, 0.0920, equivalent reflections were merged. The linear absorption coefficient, μ, for Mo-Kα radiation of 3.960 mm-1 was applied, which resulted in transmission factors ranging from 0.4898 to 0.6740. The data were corrected for Lorentz and
- [29] Final R factors, R1 and wR2 are 0.0507 and 0.0825 for 20546 reflections with I> 2.0σ(I), respectively. R1 and wR2 for all data are 0.0771 and 0.0891 for 26544 reflections. The number of parameters was 964. GOF values are 1.045 for I> 2.0σ(I) and 1.045 for all data, respectively.

69
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71
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72
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73
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74
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75
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76
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77
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78
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79
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80
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81
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82
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83
- 85163245124
- Crystal data for 5c·4C4H8O: Fw, 2257.92 (0.33 X 0.17 X 0.10 mm, triclinic, space group P1, 2, a, 14.5331(4, b, 17.0949(6, c, 21.0655(6) Å, α, 70.6216(8, β, 70.4231(10, γ, 72.5510(10)°, V, 4545.7(2) A3, Z, 2, calculated density, 1.650 Mg/m 3. Data were collected with Rigaku RAXIS RAPID imaging plate area detector with graphite monochromated Mo-Kα radiation at a temperature of 100(2) K to a maximum 2θ value of 61.0°. A total of 270 oscillation images were collected. Of the 80453 reflections that were collected, 27259 were unique Rint, 0.1024, equivalent reflections were merged. The linear absorption coefficient, μ, for Mo-Kα radiation of 3.514mm-1 was applied, which resulted in transmission factors ranging from 0.4844 to 0.7049. The data were corre
- [29] Final R factors, R11 and wR2 are 0.0645 and 0.1456 for 20608 reflections with I>2.0σ(I), respectively. R1 and wR2 for all data are 0.0926 and 0.1585 for 27259 reflections. The number of parameters was 964. GOF values are 1.028 for I> 2.0σ(I) and 1.028 for all data, respectively. CCDC-620212 and 620213 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

84
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85
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86
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- P. T. Beurskens, G. Beurskens, R. de Gelder, S. Garcia-Granda, R. O. Gould, R. Israel, J. M. M. Smits, The DIRDIF-99 Program System (version 99.2), Crystallography Laboratory, University of Nijmegen, The Netherlands, 1999.

87
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- Beurskens, P.T.¹ Admiraal, G.² Behm, H.³ Beurskens, G.⁴ Smits, J.M.M.⁵ Smykalla, C.⁶

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