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33846282521
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Zn (4c, C61H47.24Cl1N 13O10Zn2.38) and (C61H 47.77Cl1N13O10Zn2.11) plus disordered solvent, Mo Kα radiation, T, 150 K, trigonal, P31, a, 32.195(2) Å, c, 12.584(1) Å, V, 11296.2(13) Å3, Z, 326 254 unique reflections, R1(F, 0.088, wR2(F2, 0.219 (all data, A merohedral twin law (TWIN 010/100/00-1) was used in the final refinement cycles, and the fracion of this twin component was refined to 0.0821
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2) = 0.219 (all data). A merohedral twin law (TWIN 010/100/00-1) was used in the final refinement cycles, and the fracion of this twin component was refined to 0.082(1).
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