Solid-state 17O NMR in carbohydrates

Chemical Physics Letters

Volumn 434, Issue 4-6, 2007, Pages 312-315

  Sefzik, T H ^a   Houseknecht, J B ^b   Clark, T M ^a   Prasad, S ^a   Lowary, T L ^c   Gan, Z ^d   Grandinetti, P J ^a  

^a OHIO STATE UNIVERSITY   (United States)

^b WITTENBERG UNIVERSITY   (United States)

^c UNIVERSITY OF ALBERTA   (Canada)

^d FLORIDA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

MAGNETIC FIELD EFFECTS; MOLECULAR ORIENTATION; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; OXYGEN; RATE CONSTANTS;

ASYMMETRY PARAMETERS; METHYL GLUCOSIDES; NUCLEAR MAGNETIC RESONANCE MEASUREMENT; QUADRUPOLAR COUPLING CONSTANTS;

CARBOHYDRATES;

EID: 33846217800     PISSN: 00092614     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cplett.2006.12.008     Document Type: Article

References (24)

1. Lemaître V., de Planque M.R.R., Howes A.P., Smith M.E., Dupree R., and Watts A. J. Am. Chem. Soc. 126 (2004) 15320
2. Hu J., Chekmenev E.Y., Gan Z., Gor'kov P.L., Saha S., Brey W.W., and Cross T.A. J. Am. Chem. Soc. 127 (2005) 11922
3. Kintzinger J.-P. Oxygen NMR. Characteristic parameters and applications. NMR, Basic Principles and Progress vol. 17 (1981), Springer-Verlag 1
4. Gerothanassis I.P., and Lauterwein J. J. Magn. Reson. 48 (1982) 431
5. Jerschow A. Prog. NMR Spect. 46 (2005) 63078
6. Lemaître V., Smith M.E., and Watts A. Solid State Nucl. Mag. 26 (2004) 215
7. Prasad S., Kwak H.T., Clark T., and Grandinetti P.J. J. Am. Chem. Soc. 124 18 (2002) 4964
8. D'Souza F.W., and Lowary T.L. J. Org. Chem. 63 (1998) 3166
9. Grandinetti P.J., Baltisberger J.H., Llor A., Lee Y.K., Werner U., Eastman M.A., and Pines A. J. Magn. Reson. A 103 (1993) 72
10. Cheng C.P., and Brown T.L. J. Am. Chem. Soc. 101 9 (1979) 2327
11. Poplett I.J.F., and Smith J.A.S. J. Chem. Soc., Faraday Trans. 2 75 (1979) 1703
12. Machida Y., Kuroki S., Kanekiyo M., Kobayashi M., Ando I., and Amiya S. J. Mol. Struct. 554 (2000) 81
13. Aguilar A.R., and Guareno E.O. J. Chem. Thermodyn. 32 (2000) 767
14. Liu F., Phung C.G., Alderman D.W., and Grant D.M. J. Am. Chem. Soc. 118 (1996) 10629
15. Unfortunately, the MAS probe rotor axis angle at 19.6 T was misset by approximately 2.76°. Rather than redo experiments, we included the rotor axis angle as a fit parameter in our lineshape analyses. All fits converged on a rotor angle of 57.5 ± 0.1°.
16. Schramm S., and Oldfield E. J. Am. Chem. Soc. 106 (1984) 2502
17. Clark T.M., and Grandinetti P.J. Solid State Nucl Mag 16 (2000) 55
18. Clark T.M., and Grandinetti P.J. J. Phys.-Condens. Mat. 15 (2003) S2387
19. Clark T., Grandinetti P.J., Florian P., and Stebbins J. Phys. Rev. B 70 (2004) 064202
20. M.J. Frisch et al., Gaussian 03, rev. b.05 (2003).
21. Jeffrey G.A., McMullan R.K., and Takagi S. Acta Crystallogr. B33 (1977) 737
22. Takagi S., and Jeffrey G.A. Acta Crystallogr. B 35 (1979) 902
23. Jeffrey G.A., and Takagi S. Acta Crystallogr. B 33 (1977) 738
24. Zhao X.G., Dvorak M., Silvernail C., Belot J., and Harbison G.S. Solid State Nucl. Mag. 22 2-3 (2002) 363