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Inorganic Chemistry

Volumn 45, Issue 25, 2006, Pages 10013-10015

A "turn-on" fluorescent sensor for selective HG(II) detection in aqueous media based on metal-induced dye formation

(5) Zhao, Yonggang a Lin, Zhihua a He, Cheng a Wu, Hongmei a Duan, Chunying a

a DALIAN UNIVERSITY OF TECHNOLOGY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33846178621 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic061067b Document Type: Article

Times cited : (96)

References (36)

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- Compound 1 was synthesized as follows: H2L (0.10 g, 0.23 mmol) and Hg(NO3)2·0.5H2O (0.08 g, 0.23 mmol) were mixed and stirred in 20 mL of CH3OH for 2 h at room temperature, with a red solution forming. After careful evaporation of the solution in air for a few days, orange crystals with a prism shape were formed. Anal. Calcd for Hg2C47H40N18O 8S2: C, 38.93; H, 2.78; N, 17.38. Found: C, 39.34; H, 2.92; N, 17.03
- 2: C, 38.93; H, 2.78; N, 17.38. Found: C, 39.34; H, 2.92; N, 17.03.

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- Crystal data for compound 1: C48H48Hg 2N18O12S2, Mr, 1534.34, monoclinic, space group P21/n, a, 7.676(5) Å, b, 16.301(10) Å, c, 22.599(14) Å, β, 91.42(1)°, V, 2827(3) Å3, ρcald, 1.802 Mg m-3, μ, 5.574 mm-1, Z, 2, T, 293 K, R1, 0.0579, wR2, 0.1574. The intensities of compound 1 were collected on a Siemens SMART CCD diffractometer with graphite-monochromated Mo Kα (λ, 0.710 73 Å) using the SMART and SAINT programs; 4929 unique reflections were collected for 3388 reflections with I > 2σI, The structure was solved by direct methods and refined on F2 by full-matrix least-squares methods with SHELXTL version 5.1. All of the non-H atoms were refined anisotropically
- 2 by full-matrix least-squares methods with SHELXTL version 5.1. All of the non-H atoms were refined anisotropically.

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35
- 33846180720
- For compound 2. Elem anal. Calcd for HgC25H 24N8O2Cl2: C, 40.58; H, 3.27; N, 15.14. Found: C, 40.12; H, 2.98; N, 15.37. Crystal data of compound 2: HgC23H16Cl2N8, Mr, 675.93, monoclinic, space group P21/n, a, 10.5580(10) Å, b, 14.5870(10) Å, c, 15.3600-(10) Å, β, 107.090(10)°, V, 2261.1(3) Å3, ρcald, 1.986 Mg m-3, μ, 7.074 mm-1, Z, 4, T, 298 K. A total of 4379 unique reflections were collected on a Siemens SMART CCD system, R1, 0.0462, and wR2, 0.0858 for 3145 reflections with I > 2σ7
- -1, Z = 4, T = 298 K. A total of 4379 unique reflections were collected on a Siemens SMART CCD system, R1 = 0.0462, and wR2 = 0.0858 for 3145 reflections with I > 2σ(7).

36
- 33846184168
- The compound HL was synthesized as follows: The mixture of H2L1 (0.44 g, 1 mmol) and Hg(NO3) 2·0.5H2O (0.33 g, 1 mmol) in 40 mL of CH 3OH were refluxed for 6 h. Upon the addition of 1.2 mL of NH 4S (8% aqueous solution) and further stirring for 4 h, a dark precipitate formed and was filtered off. The crude product that was obtained by evaporating the filtration under reduced pressure was chromatographed on silica gel with a CH2Cl2/MeOH (1:1) solution as the eluent. Yield: 0.18 g, 45, 1H NMR (400 MHz, DMSO-d6, δ 9.35-9.37 (H, d, J, 6.8 Hz, 9.26-9.28 (H, d, J, 8.8 Hz, 8.96-9.00 (H, t, J, 8.0 Hz, 8.83-8.84 (H, d, J, 4.8 Hz, 8.77-8.79 (H, d, J, 4.8 Hz, 8.72-8.74 (H, d, J, 8.0 Hz, 8.59-8.60 (H, d, J, 4.4 Hz, 8.39-8.43(H, t, J, 7.2 Hz, 8.13-8.16 H, t, J, 6.8
- 6): δ 9.35-9.37 (H, d, J = 6.8 Hz), 9.26-9.28 (H, d, J = 8.8 Hz), 8.96-9.00 (H, t, J = 8.0 Hz), 8.83-8.84 (H, d, J = 4.8 Hz), 8.77-8.79 (H, d, J = 4.8 Hz), 8.72-8.74 (H, d, J = 8.0 Hz), 8.59-8.60 (H, d, J = 4.4 Hz), 8.39-8.43(H, t, J = 7.2 Hz), 8.13-8.16 (H, t, J = 6.8 Hz), 8.144 (H, s, NH), 8.08-8.12 (H, t, J = 8.8 Hz), 8.00-8.02 (H, d, J = 8.0 Hz), 7.75-7.77 (H, d, J = 8.0 Hz), 7.67-7.70 (H, t, J = 6.4 Hz), 7.64-7.70 (H, t, J = 6.4 Hz). 7.56-7.59 (H, t, J = 6.0 Hz).

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