SCOPUS 정보 검색 플랫폼

Inorganic Chemistry

Volumn 45, Issue 25, 2006, Pages 10034-10036

Monohelical iron(II) and zinc(II) complexes of a (1R,2R)-cyclohexyl salen ligand with benz[a]anthryl sidearms

(3) Wiznycia, Alexander V a Desper, John a Levy, Christopher J a

a KANSAS STATE UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33846161224 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic061553z Document Type: Article

Times cited : (37)

References (38)

1
- 0037186822
- For examples see: a
- For examples see: (a) Zhu, Y.-Z.; Li, Z.-P.; Ma, J.-A.; Tang, F.-Y.; Kang, L.; Zhou, Q.-L.; Chan, A. S. C. Tetrahedron: Asymmetry 2002, 13, 161.
- (2002) Tetrahedron: Asymmetry , vol.13 , pp. 161
- Zhu, Y.-Z.¹ Li, Z.-P.² Ma, J.-A.³ Tang, F.-Y.⁴ Kang, L.⁵ Zhou, Q.-L.⁶ Chan, A.S.C.⁷

2
- 33751386415
- (b) Maruoka, K.; Murase, N.; Yamamoto, H. J. Org. Chem. 1993, 58, 2938.
- (1993) J. Org. Chem , vol.58 , pp. 2938
- Maruoka, K.¹ Murase, N.² Yamamoto, H.³

3
- 0002714666
- (c) End, N.; Pfaltz, A. Chem. Commun. 1998, 589.
- (1998) Chem. Commun , pp. 589
- End, N.¹ Pfaltz, A.²

4
- 0031802304
- (d) End, N.; Macko, L.; Margareta, Z.; Pfaltz, A. Chem. Eur. J. 1998, 4, 818.
- (1998) Chem. Eur. J , vol.4 , pp. 818
- End, N.¹ Macko, L.² Margareta, Z.³ Pfaltz, A.⁴

5
- 0031585110
- (e) Guo, C.; Qui, J.; Zhang, X.; Verdugo, D.; Larter, M. L.; Christie, R.; Kenney, P.; Walsh, P. J. Tetrahedron 1997, 53, 4145.
- (1997) Tetrahedron , vol.53 , pp. 4145
- Guo, C.¹ Qui, J.² Zhang, X.³ Verdugo, D.⁴ Larter, M.L.⁵ Christie, R.⁶ Kenney, P.⁷ Walsh, P.J.⁸

6
- 22644437825
- (f) Seitz, M.; Kaiser, A.; Stempfhuber, S.; Zabel, M.; Reiser, O. Inorg. Chem. 2005, 44, 4630.
- (2005) Inorg. Chem , vol.44 , pp. 4630
- Seitz, M.¹ Kaiser, A.² Stempfhuber, S.³ Zabel, M.⁴ Reiser, O.⁵

7
- 0040995579
- (a) Piguet, C.; Bernardinelli, G.; Hopfgartner, G. Chem. Rev. 1997, 97, 2005.
- (2005) Chem. Rev , vol.1997 , pp. 97
- Piguet, C.¹ Bernardinelli, G.² Hopfgartner, G.³

8
- 0036625261
- (b) Aspinall, H. C. Chem. Rev. 2002, 102, 1807.
- (2002) Chem. Rev , vol.102 , pp. 1807
- Aspinall, H.C.¹

9
- 0035498334
- (c) Albrecht, M. Chem. Rev. 2001, 101, 3457.
- (2001) Chem. Rev , vol.101 , pp. 3457
- Albrecht, M.¹

10
- 33748469342
- (d) Fleming, J. S.; Mann, K. L. V.; Couchman, S. M.; Jeffery, J. C.; McCleverty, J. A.; Ward, M. D. J. Chem. Soc., Dalton Trans. 1998, 2047.
- (1998) J. Chem. Soc., Dalton Trans , pp. 2047
- Fleming, J.S.¹ Mann, K.L.V.² Couchman, S.M.³ Jeffery, J.C.⁴ McCleverty, J.A.⁵ Ward, M.D.⁶

11
- 0037356210
- (e) Vázquez, M.; Bermejo, M. R.; Fondo, M.; García-Deibe, A. M.; Sanmartín, J.; Pedrido, R.; Sorace, L.; Gatteschi, D. Eur. J. Inorg. Chem. 2003, 1128.
- (2003) Eur. J. Inorg. Chem , pp. 1128
- Vázquez, M.¹ Bermejo, M.R.² Fondo, M.³ García-Deibe, A.M.⁴ Sanmartín, J.⁵ Pedrido, R.⁶ Sorace, L.⁷ Gatteschi, D.⁸

12
- 26944459962
- Wiznycia, A. V.; Desper, J.; Levy, C. J. Chem. Commun. 2005, 4693.
- (2005) Chem. Commun , pp. 4693
- Wiznycia, A.V.¹ Desper, J.² Levy, C.J.³

13
- 33846131974
- 2: C 84.86, H 5.50, N 4.50. Found: C 84.52, H 5.67, N 4.48.
- 2: C 84.86, H 5.50, N 4.50. Found: C 84.52, H 5.67, N 4.48.

14
- 28244459507
- (a) Herzfeld, R.; Nagy, P. Spectrosc. Lett. 1999, 32, 57.
- (1999) Spectrosc. Lett , vol.32 , pp. 57
- Herzfeld, R.¹ Nagy, P.²

15
- 33846176088
- (b) Császár, J. Acta Phys. Chem. 1979, 25, 129.
- (1979) Acta Phys. Chem , vol.25 , pp. 129
- Császár, J.¹

16
- 50549221532
- (c) Charette, J.; Faltlhansl, G.; Teyssie, Ph. Spectrochim. Acta 1964, 20, 597.
- (1964) Spectrochim. Acta , vol.20 , pp. 597
- Charette, J.¹ Faltlhansl, G.² Teyssie, P.³

17
- 33846167448
- Anhydrous zinc chloride (0.066 g, 0.48 mmol, sodium methoxide (0.078 g, 1.5 mmol, and (R,R)-3 (0.301 g, 0.48 mmol) were suspended into a 2:1 mixture of methylene chloride/ethanol (15 mL) and stirred for 16 h. The reaction mixture was concentrated and filtered to give a yellow solid that was subsequently dissolved into THF (20 mL) and filtered to remove fine insoluble solids. The clear filtrate was stirred for 2 h, resulting in the formation of a yellow precipitate, which was collected and washed consecutively with THF (5 mL) and ethanol (5 mL) to afford (R,R)-4 (0.177 g, 53, yield, Anal. Calcd for C44H32N2O2Zn: C 77.02, H 4.70, N 4.08. Found: C 77.19, H 4.65, N 4.21, R,R)-5 was synthesized in 68% yield by the same general procedure, with some variation in workup see Supporting Information, Anal. Calcd for C44H 32N2O2Fe: C 78.11, H 4.77, N 4.14. Found
- 2Fe: C 78.11, H 4.77, N 4.14. Found: C 78.12, H 5.02, N 3.90.

18
- 33846162829
- The sample used for crystallization was not thoroughly dried of residual solvent, and this is the source of ethanol in the crystals. Crystal data for (R,R)-4(pyridine)·[0.5C5H5N C 2H5OH, Bruker SMART 1000, yellow prisms, 0.44 x 0.24 x 0.22 mm3, C53.5H44.5N3.5O 3Zn, M, 849.80, hexagonal, a, 26.3597(6) Å, c, 10.2518(5) Å, V, 6169.0-(4) Å3, T, 100(2) K, space group P65, Z, 6, 2θ collection range 0.89-30.10°, h ± 37, k ± 36, 1 ± 14, μ(Mo Kα, 0.649 mm-1, graphite monochrometer, 71 849 reflections collected, 12 068 unique (R int, 0.0304) which were used in all calculations. R1, 0.0395 (all data) and wR2(F2, 0.0996. Flack parameter, 0.0036
- 2) = 0.0996. Flack parameter = -0.003(6).

19
- 0032761925
- Amendola, V.; Fabbrizzi, L.; Linati, L.; Mangano, C.; Pallavicini, P.; Pedrazzini, V.; Zema, M. Chem. Eur. J. 1999, 5, 3679. Racemic ligand was used; (R,R) gives M helices and (S,S) gives P helices.
- Amendola, V.; Fabbrizzi, L.; Linati, L.; Mangano, C.; Pallavicini, P.; Pedrazzini, V.; Zema, M. Chem. Eur. J. 1999, 5, 3679. Racemic ligand was used; (R,R) gives M helices and (S,S) gives P helices.

20
- 33846134760
- Single crystals suitable for X-ray analysis were grown by diffusion of ethanol into a pyridine solution of (R,R)-5. Crystal data for (R,R)-5(pyridine, Bruker SMART 1000, black prisms, 0.33 x 0.18 x 0.09 mm3, C49H37N3O2Fe, M, 755.67, monoclinic, a, 10.7342(11) Å, b, 19.595(2) Å, c, 17.7357(19) Å, b, 105.904(2)°, V, 3587.8(7) Å3, T, 100(2) K, space group P21, Z, 4, 2θ collection range 2.01-30.03°, h ± 15, k ± 27, 1 ± 24, μ(Mo Kα, 0.468 mm-1, graphite monochrometer, 41 757 reflections collected, 20 505 unique (Rint, 0.0322) which were used in all calculations. R1, 0.0539 (all data) and wR2(F2, 0.1107. Flack parameter, 0.0029
- 2) = 0.1107. Flack parameter = 0.002(9).

21
- 0004260535
- Wiley: New York
- (a) Steed, J. W.; Atwood, J. L. Supramolecular Chemistry; Wiley: New York, 2000; p 26.
- (2000) Supramolecular Chemistry , pp. 26
- Steed, J.W.¹ Atwood, J.L.²

22
- 0001227655
- (b) Hunter, C. A.; Sanders, K. M. J. Am. Chem. Soc. 1990, 112, 5525.
- (1990) J. Am. Chem. Soc , vol.112 , pp. 5525
- Hunter, C.A.¹ Sanders, K.M.²

23
- 33846173057
- B3LYP* calculations carried out using ADF showed the M conformer to be more favorable as follows (kcal/mol, R,R)-4, 1.1; (R,R)-4(py, 3.6; (R,R)-5, 1.9; (R,R)-5py, 0.1
- B3LYP* calculations carried out using ADF showed the M conformer to be more favorable as follows (kcal/mol). (R,R)-4, 1.1; (R,R)-4(py), 3.6; (R,R)-5, 1.9; (R,R)-5(py), 0.1.

24
- 0942298051
- Jiang, H.; Dolain, C.; Léger, J.-M;, Gornitzka, H.; Huc, I. J. Am. Chem. Soc. 2004, 126, 1034.
- (2004) J. Am. Chem. Soc , vol.126 , pp. 1034
- Jiang, H.¹ Dolain, C.² Léger, J.-M.³ Gornitzka, H.⁴ Huc, I.⁵

25
- 0037237230
- (a) Mazet, C.; Gade, L. H. Inorg. Chem. 2003, 42, 210.
- (2003) Inorg. Chem , vol.42 , pp. 210
- Mazet, C.¹ Gade, L.H.²

26
- 0000091652
- (b) Baum, G.; Constable, E. C.; Fenske, D.; Housecroft, C. H.; Kulke, T.; Neuburger, M.; Zehnder, M. J. Chem. Soc., Dalton Trans. 2000, 945.
- (2000) J. Chem. Soc., Dalton Trans , pp. 945
- Baum, G.¹ Constable, E.C.² Fenske, D.³ Housecroft, C.H.⁴ Kulke, T.⁵ Neuburger, M.⁶ Zehnder, M.⁷

27
- 33846169433
- 1998, 2659
- (c) 1998, 2659.

28
- 0033590547
- (d) Baum, G.; Constable, E. C.; Fenske, D.; Housecroft C. E.; Kulke, T. Chem. Commun. 1999, 195.
- (1999) Chem. Commun , pp. 195
- Baum, G.¹ Constable, E.C.² Fenske, D.³ Housecroft, C.E.⁴ Kulke, T.⁵

29
- 0032705017
- (e) Saalfrank, R. W.; Maid, H.; Hampel, F.; Peters, K. Eur. J. Inorg. Chem. 1999, 1859.
- (1999) Eur. J. Inorg. Chem , pp. 1859
- Saalfrank, R.W.¹ Maid, H.² Hampel, F.³ Peters, K.⁴

30
- 0002501216
- (f) Saalfrank, R. W.; Struck, O.; Peters, K.; von Schnering, H. G. Inorg. Chim. Acta 1994, 222, 5.
- (1994) Inorg. Chim. Acta , vol.222 , pp. 5
- Saalfrank, R.W.¹ Struck, O.² Peters, K.³ von Schnering, H.G.⁴

31
- 0001074538
- (a) Ung, Van A.; Bardwell, D. A.; Jeffery, J. C.; Maher, J. P.; McCleverty, J. A.; Ward, M. D.; Williamson, A. Inorg. Chem. 1996, 35, 5290.
- (1996) Inorg. Chem , vol.35 , pp. 5290
- Ung, V.A.¹ Bardwell, D.A.² Jeffery, J.C.³ Maher, J.P.⁴ McCleverty, J.A.⁵ Ward, M.D.⁶ Williamson, A.⁷

32
- 0042734012
- (b) Suzuki, T. M.; Ohba, S.; Sato, S.; Saito, Y.; Saito, K. Inorg. Chem. 1983, 22, 2048.
- (1983) Inorg. Chem , vol.22 , pp. 2048
- Suzuki, T.M.¹ Ohba, S.² Sato, S.³ Saito, Y.⁴ Saito, K.⁵

33
- 0001020647
- (c) Biscarini, P.; Franca, R.; Kuroda, R. Inorg. Chem. 1995, 34, 4618.
- (1995) Inorg. Chem , vol.34 , pp. 4618
- Biscarini, P.¹ Franca, R.² Kuroda, R.³

34
- 0038172172
- (a) Zhang, Y.-L.; Ruan, W.-J.; Zhao, X.-J.; Wang, H.-G; Zhu, Z.-A. Polyhedron 2003, 22, 1535.
- (2003) Polyhedron , vol.22 , pp. 1535
- Zhang, Y.-L.¹ Ruan, W.-J.² Zhao, X.-J.³ Wang, H.-G.⁴ Zhu, Z.-A.⁵

35
- 37049108291
- (b) Pasini, A.; Gullotti, M.; Ugo, R. J. Chem. Soc., Dalton Trans. 1977, 346.
- (1977) J. Chem. Soc., Dalton Trans , pp. 346
- Pasini, A.¹ Gullotti, M.² Ugo, R.³

36
- 0037114742
- (c) Szlyk, E.; Surdykowski, A.; Barwiolek;, M.; Larsen, E. Polyhedron, 2002, 21, 2711.
- (2002) Polyhedron , vol.21 , pp. 2711
- Szlyk, E.¹ Surdykowski, A.² Barwiolek, M.³ Larsen, E.⁴

37
- 0034555210
- (d) Szlyk, E.; Surdykowski, A.; Barwiolek;, M.; Larsen, E. Trans. Met. Chem. 2000, 25, 670.
- (2000) Trans. Met. Chem , vol.25 , pp. 670
- Szlyk, E.¹ Surdykowski, A.² Barwiolek, M.³ Larsen, E.⁴

38
- 33947438555
- Jones, R. N. J. Am. Chem. Soc. 1945, 67, 2127.
- (1945) J. Am. Chem. Soc , vol.67 , pp. 2127
- Jones, R.N.¹

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.