[(H2en)7(C2O4) 2]n(Pb4I18)n· 4nH2O, a new type of perovskite co-templated by both organic cations and anions

Inorganic Chemistry

Volumn 45, Issue 25, 2006, Pages 10028-10030

  Zhang, Zhang Jing ^a,b   Guo, Guo Cong ^a   Xu, Gang ^a   Fu, Ming Lai ^a   Zou, Jian Ping ^a   Huang, Jin Shun ^a  

^a FUJIAN INSTITUTE OF RESEARCH ON THE STRUCTURE OF MATTER   (China)

^b UNIVERSITY OF CHINESE ACADEMY OF SCIENCES   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33846148290     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic061555j     Document Type: Article

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31. int = 0.0292), 5500 reflections with I > 2σ(I), R1 = 0.0368, wR2 = 0.0874.
32. 2). Thermogravimetric analysis (Figure S2 in the Supporting Information) of 1 showed a weight loss of 1.7% corresponding to the loss of four water molecules in the temperature range 25-105°C, and compound 1 decomposes above 276°C. A probable process of decomposition is shown in electrospray ionization. Elem anal. Calcd for 1: C, 5.70; H, 2.07; N, 5.17. Found: C, 5.45; H, 2.25; N, 4.98. IR (KBr): 3434.65, vs; 2918, m; 1618, s; 1569, m; 1493, s; 1299, s; 1023, m; 997, m; 968, w; 772, m; 458, m.
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