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Crystallographic data for L-1: C63H 57Cl10N2O10.5S2, Mr, 1428.73, 0.35 x 0.23 x 0.16 mm3, trigonal, a, 26.6288(5, b, 26.6288(5, c, 9.0055(1) Å, V= 5530.21(16) Å3, space group P3(1, Z, 3, ρcalcd, 1.287, λ(MoKα, 0.71073 Å, T, 120(2) K, 26669 reflections, 8429 unique 8390 observed, Rint, 0.0426, R 1, 0.0875, ωR2, 0.2437, for 775 parameters and 19 restraints
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2 = 0.2437, for 775 parameters and 19 restraints.
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33846079080
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The sharpness of the peaks in may be explained by rapid rotation around the long axis of the tube
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The sharpness of the peaks in may be explained by rapid rotation around the long axis of the tube.
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