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6
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-
0034685768
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-
Bowden, R. D.; Comina, P. J.; Greenhall, M. P.; Kariuki, B. M.; Loveday, A.; Philp, D. Tetrahedron 2000, 56, 3399-3408.
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(2000)
Tetrahedron
, vol.56
, pp. 3399-3408
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-
Bowden, R.D.1
Comina, P.J.2
Greenhall, M.P.3
Kariuki, B.M.4
Loveday, A.5
Philp, D.6
-
10
-
-
33750324253
-
-
Dolbier, W. R., Jr.; Ait-Mohand, S.; Schertz, T. D.; Sergeeva, T. A.; Cradlebaugh, J. A.; Mitani, A.; Gard, G. L.; Winter, R. W.; Thrasher, J. S. J. Fluorine Chem. 2006, 127, 1302-1310.
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(2006)
J. Fluorine Chem
, vol.127
, pp. 1302-1310
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-
Dolbier Jr., W.R.1
Ait-Mohand, S.2
Schertz, T.D.3
Sergeeva, T.A.4
Cradlebaugh, J.A.5
Mitani, A.6
Gard, G.L.7
Winter, R.W.8
Thrasher, J.S.9
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12
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-
33646435834
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-
Kirsch, P.; Binder, J. T.; Lork, E.; Roschenthaler, G. V. J. Fluorine Chem. 2006, 127, 610-619.
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(2006)
J. Fluorine Chem
, vol.127
, pp. 610-619
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-
Kirsch, P.1
Binder, J.T.2
Lork, E.3
Roschenthaler, G.V.4
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14
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-
33845989594
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-
5,16
-
5,16
-
-
-
-
17
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-
33845983052
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-
5Cl. The exo- and endo-adducts could be readily separated by silica gel chromatography
-
5Cl. The exo- and endo-adducts could be readily separated by silica gel chromatography
-
-
-
-
18
-
-
33846001113
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-
2a: 1H NMR, δ 2.10-2.38 (m, 2H, CH2, 3.53 (dd, J, 8.7, 5.1 Hz, 1H, CH(CN, 3.74-3.90 (m, 1H, CH(SF5, 4.76 (dd, J, 5.1 Hz, 1H, CHCl, 4.96 (d, J, 5.3 Hz, 1H, bridgehead-CH, 5.27 (d, J, 5.3 Hz, 1H, bridgehead-CH, 19F NMR, δ +58.9 (d, J, 152 Hz, 4F, 81.5 (pent, J, 152 Hz, 1F, 2b: 1H NMR, δ 2.10-2.38 (m, 1H, 2.77 (dd, J, 13.5, 9.0 Hz, 1H, 2.91 (dd, J, 9.0, 3.9 Hz, 1H, CHCN, 3.74-3.90 (m, 1H, CHSF5, 4.72 (t, J, 5.1 Hz, 1H, CHCl, 4.87 (t, J, 5.3 Hz, 1H, bridgehead-CH, 5.32 (s, 1H, bridgehead-CH, 19F NMR, δ +59.6 (d, J, 153 Hz, 4F, 81.3 (pent, J, 153 Hz, 1F, Anal, mixture of 2a and 2b) calcd for C7H 7F5ClNOS: C, 29.64; H, 2.49; N, 4.94. Found: C, 29.95; H, 2.29; N, 4.71. 3a: 1H NMR, δ 2.11 dd, J, 12.0
-
+ = 193.9841; found, 193.9850.
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-
-
-
19
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-
33846029254
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5OS: C, 28.85; H, 2.42. Found: C, 29.00; H, 2.19.
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5OS: C, 28.85; H, 2.42. Found: C, 29.00; H, 2.19.
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-
-
-
20
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0038813821
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-
Clark, J. S.; Marlin, F.; Nay, B.; Wilson, C. Org. Lett. 2003, 5, 89-92.
-
(2003)
Org. Lett
, vol.5
, pp. 89-92
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-
Clark, J.S.1
Marlin, F.2
Nay, B.3
Wilson, C.4
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21
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0031562418
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Wong, M. K.; Leung, C. Y.; Wong, H. N. C. Tetrahedron 1997, 53, 3497-3512.
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(1997)
Tetrahedron
, vol.53
, pp. 3497-3512
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-
Wong, M.K.1
Leung, C.Y.2
Wong, H.N.C.3
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22
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21844485616
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Stetinova, J.; Lesko, J.; Dandarova, M.; Kada, R.; Koren, R. Coll. Czech. Chem. Commun. 1994, 59, 2721-2726.
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(1994)
Coll. Czech. Chem. Commun
, vol.59
, pp. 2721-2726
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-
Stetinova, J.1
Lesko, J.2
Dandarova, M.3
Kada, R.4
Koren, R.5
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23
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0010816185
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Traylor, T. G.; Hill, K. W.; Tian, Z.-Q.; Rheingold, A. L.; Peisach, J.; McCracken, J. J. Am. Chem. Soc. 1988, 110, 5571-5573.
-
(1988)
J. Am. Chem. Soc
, vol.110
, pp. 5571-5573
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-
Traylor, T.G.1
Hill, K.W.2
Tian, Z.-Q.3
Rheingold, A.L.4
Peisach, J.5
McCracken, J.6
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24
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-
3142585296
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Hutton, J.; Potts, B.; Southern, P. F. Syn. Commun. 1979, 9, 789-789.
-
(1979)
Syn. Commun
, vol.9
, pp. 789-789
-
-
Hutton, J.1
Potts, B.2
Southern, P.F.3
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25
-
-
33845988138
-
-
Not having been isolated or observed indirectly, the regiochemistry of the intermediate Diels-Alder adduct cannot be known
-
Not having been isolated or observed indirectly, the regiochemistry of the intermediate Diels-Alder adduct cannot be known.
-
-
-
-
26
-
-
33846008515
-
-
+ = 231.0533, found 231.0541.
-
+ = 231.0533, found 231.0541.
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