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The original publication dates back to 1956, prior to the availability of 1H NMR. Thus, it is unclear whether the initially reported synthesis also yielded a mixture of three regioisomers that were unknowingly separated in a later step
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The original publication dates back to 1956, prior to the availability of 1H NMR. Thus, it is unclear whether the initially reported synthesis also yielded a mixture of three regioisomers that were unknowingly separated in a later step.
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15
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33846031718
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The product distribution was calculated from the integrations of the benzyl protons of each of the regioisomers in the 1H NMR spectrum. The chemical shifts of these protons in CDCl3 are: d 4.84 (2c, 4.68 (2a, and 4.59 2b
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1H NMR spectrum. The chemical shifts of these protons in CDCl3 are: d 4.84 (2c), 4.68 (2a), and 4.59 (2b).
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33845971658
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The sample was analyzed using the procedures described in ref 6
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The sample was analyzed using the procedures described in ref 6.
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