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Crystal data for 1 (C24H26Cl4O 6Ti2, C7H8) at, 120 °C: Space group P43, Z, 5, a, b, 1005.1(2) pm, c, 3329.8(2) pm, α, β, γ= 90°, V, 3.36401(19) nm3, ρ, 1.463 Mg/m3, Bruker SMART CCD diffractometer, MoKα radiation, 2θmax: 32.59, 91994 measured data, 12226 unique data, Rint, 0.0716, R1, 0.0371, Flack parameter 0.00(1, Programs used: SAINT [Bruker AXS, 1998, SADABS [Bruker AXS, 1998, SHELXS-97 [Sheldrick, 1990, SHELXL-97 [Sheldrick, 1997, Crystallographic data for the structure has been deposited with the Cambridge Crystallographic Data Centre, CCDC 299835. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 IEZ, UK (Fax: int.code, 1223)336-033; e-mail for inquiry: fileserv@ccdc.cam.ac.uk; e-mail for deposition: deposit@ccdc.cam.ac. uk
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1 = 0.0371, Flack parameter 0.00(1). Programs used: SAINT [Bruker AXS, 1998], SADABS [Bruker AXS, 1998], SHELXS-97 [Sheldrick, 1990], SHELXL-97 [Sheldrick, 1997]. Crystallographic data for the structure has been deposited with the Cambridge Crystallographic Data Centre, CCDC 299835. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 IEZ, UK (Fax: int.code+( 1223)336-033; e-mail for inquiry: fileserv@ccdc.cam.ac.uk; e-mail for deposition: deposit@ccdc.cam.ac. uk).
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