Spatial relationships between polymers in Sitka spruce: Proton spin-diffusion studies

Holzforschung

Volumn 60, Issue 6, 2006, Pages 665-673

  Altaner, Clemens ^a   Apperley, David C ^b   Jarvis, Michael C ^a  

^a UNIVERSITY OF GLASGOW   (United Kingdom)

^b DURHAM UNIVERSITY   (United Kingdom)

Author keywords

Cell wall models; Cellulose; Hemicellulose; Lignin; NMR spectroscopy; Supramolecular structure of wood

Indexed keywords

ELECTRONIC STRUCTURE; FOURIER TRANSFORM INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC POLYMERS; PROTONS;

PROTON SPIN DIFFUSION; SUPRAMOLECULAR STRUCTURE; VAPOR PHASE EXCHANGE;

SOFTWOODS;

CELL WALLS; CELLULOSE; HCS PULPING; LIGNINS; NUCLEAR MAGNETIC RESONANCE; PICEA SITCHENSIS; POLYMERS; PROTONS;

PICEA SITCHENSIS;

EID: 33845458616     PISSN: 00183830     EISSN: 1437434X     Source Type: Trade Journal    
DOI: 10.1515/HF.2006.112     Document Type: Article

References (33)

1. Ahvazi, B.C., Argyropoulos, D.S. (1999) Proton spin-lattice relaxation time measurements of solid wood and its constituents as a function of pH: Part II. Solid State Nucl. Magn. Reson. 15:49-57.
2. Akerholm, M., Salmén, L. (2004) Softening of wood polymers induced by moisture studied by dynamic FTIR spectroscopy. J. Appl. Polym. Sci. 94:2032-2040.
3. Bardet, M., Gagnaire, D., Nardin, R., Robert, D., Vincendon, M. (1986) Use of C-13 enriched wood for structural NMR investigation of wood and wood components, cellulose and lignin, in solid and in solution. Holzforschung 40:17-24.
4. Bertaud, F., Holmbom, B. (2004) Chemical composition of earlywood and latewood in Norway spruce heartwood, sapwood and transition zone wood. Wood Sci. Technol. 38:245-256.
5. Fahlén, J., Salmén, L. (2005) Pore and matrix distribution in the fiber wall revealed by atomic force microscopy and image analysis. Biomacromolecules 6:433-438.
6. Ha, M.A., Evans, B.W., Jarvis, M.C., Apperley, D.C., Kenwright, A.M. (1996) CP-MAS NMR of highly mobile hydrated biopolymers: polysaccharides of Allium cell walls. Carbohydr. Res. 288:15-23.
7. Ha, M.A., Apperley, D.C., Evans, B.W., Huxham, I.M., Jardine, W.G., Viëtor, R.J., Reis, D., Vian, B., Jarvis, M.C. (1998) Fine structure in cellulose microfibrils: NMR evidence from onion and quince. Plant J. 16:183-190.
8. Hafren, J., Fujino, T., Itoh, T. (1999) Changes in cell wall architecture of differentiating tracheids of Pinus thunbergii during lignification. Plant Cell Physiol. 40:532-541.
9. Haw, J.F., Maciel, G.E., Schroeder, H.A. (1984) Carbon-13 nuclear magnetic resonance spectrometric study of wood and wood pulping with cross polarization and magic-angle spinning. Anal. Chem. 56:1323-1329.
10. Hult, E.L., Larsson, P.T., Iversen, T. (2000) A comparative CP/MAS C-13-NMR study of cellulose structure in spruce wood and kraft pulp. Cellulose 7:35-55.
11. 13C NMR spectra of (1→4)-linked glucose polymers and oligomers: Anomeric and related effects. Carbohydr. Res. 259:311-318.
12. 1 cancellation schemes in Goldman-Shen-type experiments. Chem. Phys. Lett. 173:471-475.
13. Kim, Y.S., Newman, R.H. (1995) Solid-state C-13 NMR study of wood degraded by the brown-rot fungus Gloeophyllum trabeum. Holzforschung 49:109-114.
14. Larsson, P.T., Wickholm, K., Iversen, T. (1997) A CP/MAS C-13 NMR investigation of molecular ordering in celluloses. Carbohydr. Res. 302:19-25.
15. Larsson, P.T., Hult, E.L., Wickholm, K., Pettersson, E., Iversen, T. (1999) CP/MAS C-13-NMR spectroscopy applied to structure and interaction studies on cellulose I. Solid State Nucl. Magn. Reson. 15:31-40.
16. Liitia, T., Maunu, S.L., Hortling, B. (2000) Solid-state NMR studies of residual lignin and its association with carbohydrates. J. Pulp Paper Sci. 26:323-330.
17. Maunu, S.L. (2002) NMR studies of wood and wood products. Prog. Nucl. Magn. Reson. Spectrosc. 40:151-174.
18. Newman, R.H. (1992) Nuclear magnetic resonance study of spatial relationships between chemical components in wood cell walls. Holzforschung 46:205-210.
19. Newman, R.H. (1999) Estimation of the lateral dimensions of cellulose crystallites using C-13 NMR signal strengths. Solid State Nucl. Magn. Reson. 15:21-29.
20. Newman, R.H., Davidson, T.C. (2004) Molecular conformations at the cellulose-water interface. Cellulose 11:23-32.
21. Newman, R.H., Hemmingson, J.A. (1990) Determination of the degree of cellulose crystallinity in wood by C-13 nuclear magnetic resonance spectroscopy. Holzforschung 44:351-355.
22. Newman, R.H., Hemmingson, J.A. (1995) C-13 NMR distinction between categories of molecular order and disorder in cellulose. Cellulose 2:95-110.
23. Singh, A., Daniel, G., Nilsson, T. (2002) Ultrastructure of the S-2 layer in relation to lignin distribution in Pinus radiata tracheids. J. Wood Sci. 48:95-98.
24. Sivonen, H., Nuopponen, M., Maunu, S.L., Sundholm, F., Vuorinen, T. (2003) Carbon-13 cross-polarization magic angle spinning nuclear magnetic resonance and Fourier transform infrared studies of thermally modified wood exposed to brown and soft rot fungi. Appl. Spectrosc. 57:266-273.
25. Tekely, P., Vignon, M.R. (1987a) Cross polarization magic angle spinning C-13 NMR characterization of steam exploded poplar wood. J. Wood Chem. Technol. 7:215-228.
26. 2 relaxation times of wood components using C-13 CP MAS NMR. J. Polym. Sci. C-Polym. Lett. 25:257-261.
27. Teleman, A., Larsson, P.T., Iversen, T. (2001) On the accessibility and structure of xylan in birch kraft pulp. Cellulose 8:209-215.
28. Terashima, N., Awano, T., Takabe, K., Yoshida, M. (2004) Formation of macromolecular lignin in ginkgo xylem cell walls as observed by field emission scanning electron microscopy. C. R. Biol. 327:903-910.
29. Viëtor, R.J., Newman, R.H., Ha, M.A., Apperley, D.C., Jarvis, M.C. (2002) Conformational features of crystal-surface cellulose from higher plants. Plant J. 30:721-731.
30. Wickholm, K., Larsson P.T., Iversen, T. (1998) Assignment of non-crystalline forms in cellulose I by CP/MAS C-13 NMR spectroscopy. Carbohydr. Res. 312:123-129.
31. Wickholm, K., Hult, E.L., Larsson, P.T., Iversen, T., Lennholm, H. (2001) Quantification of cellulose forms in complex cellulose materials: A chemometric model. Cellulose 8:139-148.
32. Wikberg, H., Maunu, S.L. (2004) Characterisation of thermally modified hard- and softwoods by C-13 CPMAS NMR. Carbohydr. Polym. 58:461-466.
33. Zhang, S., Mehring, M. (1989) A modified Goldman-Shen NMR pulse sequence. Chem. Phys. Lett. 160:644.