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For syntheses of substituted bullvalenes from the parent compound, see: (a) Sarma, K.; Witt, W.; Schröder, G. Chem. Ber. 1986, 119, 2339-2349.
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(b) Bullvalene-crown ether: Sarma, K.; Witt, W.; Schröder, G. Chem. Ber. 1983, 116, 3800-3812.
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(c) Pentabromobullvalene and hexabromobullvalene: Rebsamen, K.; Schröder, G. Chem. Ber. 1993, 126, 1425-1427.
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33845190043
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(d) Tetramethylbullvalene and hexamethylbibullvalene: Rebsamen, K.; Schröder, G. Chem. Ber. 1993, 126, 1419-1423.
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0029836176
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see
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For recent studies of monosubstituted bullvalenes, see: (a) Poupko, R.; Zimmermann, H.; Müller, K.; Luz, Z. J. Am. Chem. Soc. 1996, 118, 7995-8005.
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(b) Luz, Z.; Olivier, L.; Poupko, R.; Muller, K.; Krieger, C.; Zimmermann. H. J. Am. Chem. Soc. 1998, 120, 5526-5538.
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26844462841
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see
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For rational syntheses of bullvalene, see: (a) Font, J.; López, F.; Serratosa, F. Tetrahedron Lett. 1972, 13, 2589-2590.
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33845228866
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Ref 4e
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(b) Ref 4e.
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(b) Griffith, W. P.; Jolliffe, J. M.; Ley, S. V.; Springhorn, K. F.; Tiffin, P. D. Synth. Commun. 1992, 22, 1967-1971.
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Aggarwal, V. K.; Smith, H. W.; Hynd, G.; Jones, R. V. H.; Fieldhouse, R.; Spey, S. E. J. Chem. Soc., Perkin Trans. 1 2000, 3267-3276.
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Fieldhouse, R.5
Spey, S.E.6
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25
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0001564353
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For examples of acylation of sulfonium ylides, see: (a) Ratts, K. W.; Yao, A, N. J. Org. Chem. 1966, 31, 1689-1693.
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10944228332
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(b) Ziegler, E.; Wittmann, H.; Sterk, H. Monatsh. Chem. 1987, 118, 115-125.
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28
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33845219325
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note
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3 in EtOH.
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