Formation of Si-H groups during the functionalization of mesoporous silica with Grignard reagents

Microporous and Mesoporous Materials

Volumn 98, Issue 1-3, 2007, Pages 115-122

  Ramírez, Alejandro ^a,b   Sierra, Ligia ^a   Lebeau, Bénédicte ^c   Guth, Jean Louis ^c  

^a UNIVERSIDAD DE ANTIOQUIA   (Colombia)

^b UNIVERSIDAD NACIONAL DE COLOMBIA   (Colombia)

^c Ecole Nationale Superieure de Chimie de Mulhouse   (France)

Author keywords

Grignard reaction; Halogenated mesoporous silica; Hydrosilane groups; Mesoporous silica; Surface modification

Indexed keywords

CHEMICAL BONDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SILANES; SILICA; SURFACE TREATMENT; THERMOANALYSIS;

GRIGNARD REACTION; HYDROSILANE GROUPS; MESOPOROUS SILICA;

MESOPOROUS MATERIALS;

CHEMICAL BONDS; MESOPOROUS MATERIALS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SILANES; SILICA; SURFACE TREATMENT; THERMOANALYSIS;

EID: 33845187616     PISSN: 13871811     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.micromeso.2006.08.021     Document Type: Article

References (26)

1. Sadasivan S., Khushalani D., and Mann S. J. Mater. Chem. 13 (2003) 1023
2. Lebeau B., Fowler C.E., Mann S., Farcet C., Charleux B., and Sanchez C. J. Mater. Chem. 10 (2000) 2105
3. Karch K., Sebastian I., and Halasz I. J. Chromatogr. 122 (1976) 3
4. Sierra L., Lopez B., Ramírez A., and Guth J.-L. In: Galarneau A., Di Renzo F., Fajula F., and Vedrine J. (Eds). Zeolites and mesoporous materials at the dawn of the 21st century. Studies in Surface Science and Catalysis vol. 135 (2001), Elsevier, Amsterdam in CD with reference 18-P-06
5. Sander L.C., and Wise S.A. Anal. Chem. 56 (1984) 504
6. Buszewski B., Jerzierska M., Welniak M., and Berek D. J. High Resol. Chromatogr. 21 (1998) 267
7. Clark J.H., and Williamson C.J. J. Mater. Chem. 3 (1993) 575
8. Wartmann J., and Deuel H. Helv. Chim. Acta 42 (1959) 1166
9. Sandoval J.E., and Pesek J.J. Anal. Chem. 61 (1989) 2067
10. Locke D.C., Schmermund J.T., and Banner B. Anal. Chem. 44 (1972) 90
11. Pesek J.J., and Swedberg S.A. J. Chromatogr. 361 (1986) 83
12. Kang K.-K., and Rhee H.-K. In: Galarneau A., Di Renzo F., Fajula F., and Vedrine J. (Eds). Zeolites and mesoporous materials at the dawn of the 21st century. Studies in Surface Science and Catalysis vol. 135 (2001), Elsevier, Amsterdam in CD with reference 29-P-09
13. Yamamoto K., and Tatsumi T. Micropor. Mesopor. Mater. 44-45 (2001) 459
14. Heeribout L., d'Espinose de la Caillerie J.B., Legrand A.P., and Mignani G. J. Colloid Interf. Sci. 215 (1999) 296
15. Morterra C., and Low M.J.D. J. Phys. Chem. 73 (1969) 327
16. Barabash R.M., Zaitsev V.N., Kovalchuk T.V., Sfihi H., and Fraissard J. J. Phys. Chem. B 107 (2003) 4497
17. E. Chatelain-Klock, Ph.D. thesis, Ecole Nationale Superieure de Chimie de Mulhouse, Université de Haute Alsace, 1995.
18. Iler R.K. The Chemistry of Silica (1979), John Wiley and Sons, New York
19. Duke C., Miller J., Clark J., and Kybett A. Spectrochim. Acta Part A 46 (1990) 1381
20. Maciel G.E., and Ellis P.D. In: Bell A.T., and Pines A. (Eds). NMR Techniques in Catalysis (1994), Marcel Dekker, New York 268
21. Hommel H. In: Legrand A.P. (Ed). The Surface Properties of Silicas (1998), John Wiley and Sons, New York
22. Nawrocki J. J. Chromatogr. A 779 (1997) 29
23. Landmesser H., Kosslick H., Storek W., and Fricke R. Solid State Ionics 101-103 (1997) 271
24. Tuulmets A., Nguyen B.T., Panov D., Sassian M., and Jarv J. J. Org. Chem. 68 (2003) 9933
25. Cannon K.C., and R Krow G. In: Silverman G.S., and Rakita P.E. (Eds). Handbook of Grignard Reagents (1996), Marcel Dekker, New York
26. Tuulmets A., Nguyen B.T., and Panov D. J. Org. Chem. 69 (2004) 5071