Synthesis, Characterization, and Magnetic Properties of μ-oxalato- and μ-oxamido-bridged Copper(ii) Dimers: Crystal and Molecular Structures of [cu2(mepirizole)2(c2o4)(h2o)2](pf6)2⋅mepirizole⋅3h2o and [cu2(mepirizole)2(c2o4)(no3)2(h2o)]2[cu2(mepirizole)2(c2o4)(no3)2]

Inorganic Chemistry

Volumn 28, Issue 17, 1989, Pages 3378-3386

  Soto, L ^a   Garcia, J ^a   Escriva, E ^a   Legros, J P ^b   Tuchagues, J P ^b   Dahan, F ^b   Fuertes, A ^c  

^a UNIVERSITY OF VALENCIA   (Spain)

^b LCC LABORATOIRE DE CHIMIE DE COORDINATION   (France)

^c INSTITUT DE CIÈNCIA DE MATERIALS DE BARCELONA ICMAB CSIC   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33845184402     PISSN: 00201669     EISSN: 1520510X     Source Type: Journal    
DOI: 10.1021/ic00316a028     Document Type: Article

References (41)

1. Willett, R. D., Gatteschi, D., Kahn, O. Eds. Magneto-structural Correlations in Exchange-Coupled Systems; NATO ASI Series; Reidel: Dordrecht, Holland, 1985.
2. Kahn, O. Angew. Chem., Int. Ed. Engl. 1985, 24, 834–850.
3. Murray, K. S. In Biological and Inorganic Copper Chemistry; Carlin, K. D., Zubieta, J., Eds.; Academic Press, New York, 1986; Vol. 2.
4. Chariot, M. F.; Kahn, O.; Chaillet, M.; Larrieu, C. J. Am. Chem. Soc. 1986, 108, 2574–2581.
5. Takabataka, E.; Kodama, R.; Tanaka, Y.; Dohmori, R.; Tachizanawa, H.; Naito, P. Chem. Pharm. Bull. 1970, 18, 1900.
6. Molla, M. C.; Garcia, J.; Borras, J.; Foces, C.; Cano, F. H.; Martinez, M. Transition Met. Chem. (Weinheim, Ger.) 1985, 10, 460–463. Soto, L.; Legros, J. P.; Molla, M. C.; Garcia, J. Acta Crystallogr. 1987, C43, 834–836. Suarez-Varela, J.; Soto, L.; Legros, J. P.; Esteve, C.; Garcia, J. Polyhedron 1988, 7, 229–234.
7. Tormos, J. G.; Molla, M. C.; Garcia, J. Synth. React. Inorg. Met.-Org. Chem. 1986, 16, 821–829.
8. Main, P.; Hull, S. E.; Lessinger, L.; Germain, G.; Declercq, J. P.; Woolfson, M. H. “MULTAN 78, a System of Computer Programs for the Automatic Solution of Crystal Structures from X-ray Diffraction Data” Universities of York, England, and Louvain, Belgium, 1978.
9. Sheldrick, G. M. “SHELXS-86, Program for Crystal Structure Solution”: University of Gottingen, 1986.
10. Sheldrick, G. M. “SHELX, a Program for Crystal Structure Solution” University Chemical Laboratory: Cambridge, England, 1976.
11. Johnson, C. K. “ORTEP” Report ORNL-3794; Oak Ridge National Laboratory: Oak Ridge, TN, 1965.
12. International Tables for X-ray Crystallography; Kynoch: Birmingham, England, 1974.
13. Howells, E. R.; Phillips, D. C.; Rogers, D. Acta Crystallogr. 1950, 3, 210–213.
14. Luneau, D.; Savariault, J. M.; Cassoux, P.; Tuchagues, J. P. J. Chem. Soc., Dalton Trans. 1988, 1225–1235.
15. Chandler, J. P. Quantum Chemistry Program Exchange, Indiana University, Program 66.
16. Mabad, B.; Cassoux, P.; Tuchagues, J. P.; Hendrickson, D. N. Inorg. Chem. 1986, 25, 1420–1431.
17. Armendarez, P. X.; Nakamoto, K. Inorg. Chem. 1966, 5, 796–800. and references therein. Verdaguer, M.; Kahn, O.; Julve, M.; Gleizes, A. Now J. Chim. 1985, 9, 325–334.
18. Procter, I. M.; Hathaway, B. J.; Nicholls, P. J. Chem. Soc. A 1968, 1678–1684.
19. Fitzgerald, W.; Foky, J.; McSweeney, D.; Ray, N.; Sheahan, D.; Tyagi, S.; Hathaway, B.; O'Brien, P. J. Chem. Soc., Dalton Trans. 1982, 1117–1121.
20. Bencini, A.; Fabretti, A. C.; Zanchini, C.; Zannini, P. Inorg. Chem. 1987, 26, 1445–1449.
21. Muetterties, E. L.; Guggenberger, L. J. J. Am. Chem. Soc. 1974, 96, 1748–1756.
22. Hathaway, B. J. Struct. Bonding 1984, 57, 55-118.
23. Lever, A. B. P. Inorganic Electronic Spectroscopy, 2nd ed.; Elsevier: Amsterdam, The Netherlands, 1986.
24. Nakamoto, R. Infrared and Raman Spectra of Inorganic and Coordination Compounds, 4th ed.; Wiley: New York, 1986.
25. Bleaney, B.; Bowers, K. D. Proc. R. Soc. London, A 1952, 214, 451-465.
26. Journaux, Y.; Sletten, J.; Kahn, O. Inorg. Chem. 1985, 24, 4063-4069.
27. O'Connor, C. Prog. Inorg. Chem. 1982, 20, 203-283.
28. Ginsberg, A. P.; Martin, R. L.; Brookes, R. W.; Sherwood, R. C. Inorg. Chem. 1972, 11, 2884-2889.
29. Kahn, O.; Chariot, M. F. Nouv. J. Chim. 1980, 10, 567-570. Kahn, O. Inorg. Chim. Acta 1982, 62, 3-14.
30. Julve, M.; Verdaguer, M.; Kahn, O.; Gleizes, A.; Philoche-Levisalles, M. Inorg. Chem. 1983, 22, 368-370.
31. Julve, M.; Verdaguer, M.; Gleizes, A.; Philoche-Levisalles, M.; Kahn, O. Inorg. Chem. 1984, 23, 3808-3818.
32. Julve, M.; Verdaguer, M.; Chariot, M. F.; Kahn, O,; Claude, R. Inorg. Chim. Acta 1984, 82, 5-12.
33. Julve, M.; Faus, J.; Verdaguer, M.; Gleizes, A. J. Am. Chem. Soc. 1984, 106, 8306-8308.
34. Bencini, A.; Benelli, C.; Gatteschi, D.; Zanchini, C.; Fabretti, A. C.; Franchini, G. C. Inorg. Chim. Acta 1984, 86, 169-172.
35. Kahn, O.; Briat, B. J. Chem. Soc., Faraday Trans. 2 1976, 72, 268-281, 1441-1446. Girerd, J.-J.; Chariot, M. F.; Kahn, O. Mol. Phys. 1977, 34, 1063-1076.
36. Tola, P.; Kahn, O.; Chauvel, C.; Coudanne, H. Nouv. J. Chim. 1977, 1, 467-473.
37. Girerd, J.-J.; Jeannin, S.; Jeannin, Y.; Kahn, O. Inorg. Chem. 1978, 17, 3034-3040. Chauvel, C.; Girerd, J.-J.; Jeannin, Y.; Kahn, O.; Lavigne, G. Inorg. Chem. 1979, 18, 3015-3020.
38. Bencini, A.; Di Vaira, M.; Fabretti, A. C.; Gatteschi, D.; Zanchini, C. Inorg. Chem. 1984, 23, 1620-1623
39. Felthouse, T. R.; Laskowski, E. J.; Hendrickson, D. N. Inorg. Chem. 1977, 16, 1077-1089.
40. Sonnenfroh, D.; Kreilick, R. W. Inorg. Chem. 1980, 19, 1259-1262.
41. Slichter, C. P. Phys. Rev. 1955, 99, 479-480.