1,15-Bis-(2′,2′,4′-trimethyl-3′-pentoxy)phthalocyanine, a trans-form nonperipheral di-substituted phthalocyanine synthesized by the 'cross condensation' method

Journal of Organometallic Chemistry

Volumn 691, Issue 23, 2006, Pages 5074-5076

  Wang, Jun Dong ^a   Lin, Mei Jin ^a   Wu, Shao Feng ^a   Lin, Yun ^a  

^a FUZHOU UNIVERSITY   (China)

Author keywords

Cross condensation; Crystal structure; Phthalocyanine

Indexed keywords

AMINES; CONDENSATION; CRYSTAL STRUCTURE; SUBSTITUTION REACTIONS; SYNTHESIS (CHEMICAL);

ALKOXY GROUPS; CROSS CONDENSATION; PHTHALOCYANINES;

ORGANOMETALLICS;

EID: 33750351254     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jorganchem.2006.08.066     Document Type: Short Survey

References (10)

1. Wang J.D., Huang J.L., Xu X.Z., Cai J.W., and Chen N.S. Chineses J. Struct. Chem. 5 (2004) 516-519
2. Lin M.J., Wang J.-D., and Chen N.-S. Z. Anorg. Allg. Chem. 631 (2005) 1352-1354
3. Yang L., Lin M.J., Zhu X.L., Xu X.Z., and Wang J.D. J. Mol. Catal. A: Chem. 253 (2006) 25-29
4. Young J.G., and Onyebuagu W. J. Org. Chem. 55 (1990) 2155-2159
5. 1 = 0.0990 for 8240 reflections with I > 2σ(I).
6. 3)δ: 9.213, 7.993, 7.676 (m, m, m, 14H, H-Pc), 4.759 ( m, 2H, -CH -O), 2.608 (m, 2H, -CH-), 1.346-1.318( t, 12H, -C(CH3)2), 1.507-1.496(s, 18H, -C(CH3)3), -1.423 (m, 2H, H-N). MS: m/z (M+) 772.0, 1542.4 (aggregated molecular pair); UV-vis-near IR (Q band, toluene, nm): 679, 714.
7. J.G. Young, PhD thesis, Clemson University, 1987.
8. X.Z. Xu, J.D. Wang, N.S. Chen, in: The Second national Conference on Porphyrins and Phthalocyanines. Jinan, China, 2002, pp. 10-11.
9. Lin M.J., Wang J.D., Chen N.S., and Huang J.L. Inorg. Chem. Commun. 8 (2005) 900-902
10. Morley J.O., and Charlton M.H. J. Phys. Chem. 99 (1995) 1928-1934