Aerosol synthesis of hollow spherical morphology boron nitride particles

Chemistry of Materials

Volumn 18, Issue 20, 2006, Pages 4716-4718

  Wood, Gary L ^a   Paine, Robert T ^b  

^a VALDOSTA STATE UNIVERSITY   (United States)

^b NATIONAL SCIENCE FOUNDATION   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

GASTIGHT END CAPS; HEATED NULLITIES; ULTRASONIC AGITATION;

AEROSOLS; AMMONIA; DECOMPOSITION; FLOW CONTROL; POWDERS; SOLVENTS;

CUBIC BORON NITRIDE;

EID: 33750308027     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm0602601     Document Type: Article

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31. 3/DMF tend to deposit boric acid during extended runs because of evaporation of DMF. This is avoided by use of less than saturated solutions.
32. 2O system encounter water from the same sources, but the dominate source is from solvent water.
33. z (1400°C) C, 0.15; H, 1.88; B, 33.22; N, 39.10; O, 11.3 wt %. Analyses for calcined powders are represented by the example as follows: C, 0.17; H, 0.30; B, 40.40; N, 53.42; O, 2.5.
34. z materials fall in the ranges C, 0.1 -1.5 wt %, and H, 0.9-2.2 wt %, respectively. The calcined samples show ranges C, 0.5 to trace wt %, and H, 1.0 to trace wt %, respectively.
35. 3 and appearance of BO-H stretching modes in IR spectra.