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Volumn 18, Issue 44, 1977, Pages 3875-3878

A facile procedure for the synthesis of α,β-unsaturated aldehydes by three carbon homologation

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Indexed keywords


EID: 33750185682     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(01)83378-5     Document Type: Article
Times cited : (24)

References (16)
  • 1
    • 0001800728 scopus 로고
    • For some recent methods of three carbon homologation of carbonyl compounds to aldehydes see
    • (1975) Tetrahedron Lett. , pp. 3685
    • Corey1    Ulrich2
  • 2
    • 84918293301 scopus 로고
    • DMSO OXIDATION Of CYCLOPROPYLMETHANOLS WITH REARRANGEMENTS. THREE CARBON CHAIN EXTENTION OF ALDEHYDES TO α,β-UNSATURATED ALDEHYDES
    • (1976) Chemistry Letters , pp. 1297
    • Nishida1    Kataoka2
  • 6
    • 84944154430 scopus 로고
    • Doppelmetallierung von Benzyl- und Allylmercaptanen; das Thiobenzaldehyd- und Thioacrolein-Dianion
    • and references therein.
    • (1977) Chemische Berichte , vol.110 , pp. 1833
    • Geiss1    Seebach2    Seuring3
  • 10
    • 84918293300 scopus 로고    scopus 로고
    • 22OPBr: C, 63.94; H, 5.37. Found: C, 63.76; H, 5.21.
  • 12
    • 84918293299 scopus 로고    scopus 로고
    • All compounds were adequately characterized by spectral methods (IR, NMR and MS), and all new compounds gave satisfactory high resolution mass spectral and/or combustion analytical data.
  • 13
    • 84916064665 scopus 로고
    • Progress in Organic Synthesis Based on 1-Alkoxydienes and 1-Alkoxypolyenes
    • For a review of the use of 1-alkoxybutadienes in organic synthesis see
    • (1969) Russian Chemical Reviews , vol.38 , pp. 237
    • Makin1
  • 14
    • 84918293298 scopus 로고    scopus 로고
    • Other experiments have shown that the ylid 4 also reacts with other α,β-unsaturated ketones such as 3-penten-2-one and 1-acetylcyclohexene predominantly at the α-carbon.
  • 15
    • 84918293297 scopus 로고    scopus 로고
    • Hydrolysis under a variety of milder reaction conditions failed to give any appreciable amount of the β,γ-isomer.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.