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note
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To assess the influence of the workup on the E/Z ratio, 3 was allowed to react with 2a and the products were isolated via conventional aqueous workup; 3a was isolated in a somewhat lower 75% yield in a nearly identical E/Z ratio of 78:22 (compared to 77:23, Table 1, entry 1).
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30
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33750089499
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f 3b = 0.36.
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