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Angewandte Chemie International Edition in English

Volumn 31, Issue 1, 1992, Pages 93-95

Crystal and Solution Structures of the Novel Complex of Sodium Ketimide with Two Ketimine Ligands [(tBu2C = NNa)4(HN = CtBu2)2]: Stacking of Complexed and Uncomplexed (NNa)2 Rings to give a Highly Distorted (NNa)4 Cubane

(4) Clegg, William b MacGregor, Murray a Mulvey, Robert E a O'Neil, Paul A b

a UNIVERSITY OF STRATHCLYDE (United Kingdom)

b NEWCASTLE UNIVERSITY (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33749107549 PISSN: 05700833 EISSN: 15213773 Source Type: Journal
DOI: 10.1002/anie.199200931 Document Type: Article

Times cited : (10)

References (12)

1
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- Such reports were usually published by Wade et al. For a detailed list of examples see ref. [2], p. 168.

2
- 0001021357
- This review focuses on the ring stacking of organonitrogen lithium compounds
- (1991) Chem. Soc. Rev. , vol.20 , pp. 167
- Mulvey, R.E.¹

3
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- J. Chem. Soc. Dalton Trans.
- (1987) , pp. 1071
- Armstrong, D.R.¹ Barr, D.² Snaith, R.³ Clegg, W.⁴ Mulvey, R.E.⁵ Wade, K.⁶ Reed, D.⁷

4
- 37049066398
- Two mixed lithium‐sodium ketimides have been described:, J. Chem. Soc. Chem. Commun.
- (1986) , pp. 1740
- Clegg, W.¹ Mulvey, R.E.² Snaith, R.³ Toogood, G.E.⁴ Wade, K.⁵

5
- 0346616272
- J. Chem. Soc. Chem. Commun.
- (1989) , pp. 57
- Barr, D.¹ Clegg, W.² Mulvey, R.E.³ Snaith, R.⁴

6
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- (1934) J. Am. Chem. Soc. , vol.56 , pp. 2095
- Smith, G.E.P.¹ Bergstrom, F.W.²

7
- 0001563905
- (1967) J. Organomet. Chem. , vol.9 , pp. 231
- Chan, L.‐H.¹ Rochow, E.G.²

8
- 37049079419
- Ether, pentamethyldiethylenetriamine (PMDETA), pyridine, tetramethyl‐ethylenediamine (TMEDA), and triethylamine fail to give solid adducts, though a 1:1 adduct is formed with the exceptionally strong donor hexamethylphosphoramide (HMPA)., J. Chem. Soc. Dalton Trans.
- (1987) , pp. 2141
- Barr, D.¹ Snaith, R.² Clegg, W.³ Mulvey, R.E.⁴ Wade, K.⁵

9
- 84989532389
- n. M.p. 178–180°C (decomp.).

10
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- Tetrahedron Lett.
- (1966) , pp. 257
- Lochmann, L.¹ Pospiŝil, J.² Lím, D.³

11
- 84989505030
- w = 0.116, S = 1.16 for 577 parameters. Further details of the crystal structure investigation can be obtained from the Director of the Cambridge Crystallographic Data Centre, University Chemical Laboratory, Lensfield Road, Cambridge, CB2 1EW (U. K.), on quoting the full journal citation.

12
- 0000500750
- (1986) J. Am. Chem. Soc. , vol.108 , pp. 462
- Williard, P.G.¹ Carpenter, G.B.²

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