DMSO-Ac2O promoted nitration of isoquinolines. One-step synthesis of 1-nitroisoquinolines under mild conditions

Journal of the Chemical Society - Perkin Transactions 1

Volumn , Issue 15, 1996, Pages 1777-1779

  Baik, Woonphil ^a   Yun, Sangmin ^a   Rhee, Jong Uk ^a   Russell, Glen A ^b  

^a Myong Ji University   (South Korea)

^b IOWA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33749100867     PISSN: 0300922X     EISSN: None     Source Type: Journal    
DOI: 10.1039/P19960001777     Document Type: Article

References (15)

1. F. W. Bergstrom and J. H. Rodda, J. Am. Chem. Soc., 1940, 62, 3030.
2. M. J. S. Dewar and N. Trinajstic, J. Chem. Soc. A, 1971, 1220.
3. H. C. Longuet-Higgins and C. A. Coulson, Trans. Faraday Soc., 1947, 43, 87.
4. M. Natsume and M. Wada, Chem. Pharm. Bull., 1972, 20, 1589.
5. H. Gilman and G. C. Gainer, J. Am. Chem. Soc., 1947, 69, 1946.
6. G. W. Kirby, S. L. Tan and B. C. Uff, J. Chem. Soc., Perkin Trans. 1, 1979, 270.
7. M. J. S. Dewar and P. M. Maitlis, J. Chem. Soc., 1957, 2521.
8. E. Hayashi, Y. Akahori and Y. Yamamoto, Yakugaku Zasshi, 1967, 87, 1342;
9. Chem. Abstr., 1968, 69, 2847.
10. E. C. Taylor, C. Tseng and J. B. Rampal, J. Org. Chem., 1982, 47, 552.
11. 2O are required to complete the reaction.
12. Only the mp and elemental analysis were given.
13. 3) 9.14 (H-1), 8.45 (H-3), 7.50 (H-4), 7.69 (H-5), 7.56 (H-6), 7.48 (H-7), 7.85 (H-8). F. Balkau and M. L. Herffernam, Austr. J. Chem., 1971, 24, 2331.
14. K. E. Pfitzner and J. G. Moffat, J. Am. Chem. Soc., 1963, 85, 3027.
15. A. Serban, USP 3930837, 1976; Chem. Abstr., 1976, 84, 180075. Structural proof was not given.