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Angewandte Chemie International Edition in English

Volumn 34, Issue 11, 1995, Pages 1209-1212

Facile Synthesis and Solid‐State Structure of a Benzylic Amide [2]Catenane

(4) Johnston, Andrew G a Leigh, David A a Pritchard, Robin J a Deegan, Michael D b

a UNIVERSITY OF MANCHESTER (United Kingdom)

b Gas Research Centre (United Kingdom)

Author keywords

catenanes; macrocycles; structure elucidation

Indexed keywords

EID: 33748720064 PISSN: 05700833 EISSN: 15213773 Source Type: Journal
DOI: 10.1002/anie.199512091 Document Type: Article

Times cited : (255)

References (22)

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- w = 0.063 for 161 parameters. All hydrogen atoms were placed in chemically reasonable positions. Further details of the crystal structure investigation may be obtained from the Director of the Cambridge Crystallographic Data Centre, 12 Union Road, GB‐Cambridge CB2 1EZ (UK), on quoting the full journal citation.

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22
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- The use of chloroform that has not been rigorously dried or contains ethanol gives lower yields of the [2]catenane and, more problematically, produces byproducts arising from the partial hydrolysis of the starting acid chloride. These are not removed in the above workup procedure. However, in this case the [2]catenane can be obtained pure by carefully washing the end product with cold chloroform.

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