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Panek, J.S.1
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P. M. Bodnar, W. S. Palmer, J. T. Shaw, J. H. Smitrovich, J. D. Sonnenberg, A. L. Presley and K. A. Woerpel, J. Am. Chem. Soc., 1995, 117, 10 575;
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C. Gibson, T. Buck, M. Walker and R. Brückner, Synlett, 1998, 201.
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32
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33748736629
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note
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3b,3h
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-
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33
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33748735285
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note
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Tin(IV) chloride mediated reaction gave rise to 2a in 58% yield.
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-
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34
-
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33748735415
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note
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2, hexane-ethyl acetate = 15:1, v/v) gave 2a (102 mg, 89%).
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-
-
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35
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33748739715
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note
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It should be noted that allyl-tert-butyldiphenylsilane which was useful for the oxetane formation was not effective for the present cyclopentane annulation; the corresponding cycloadduct was obtained in only modest yield and oxidative cleavage of the tert-butyldiphenylsilyl group was not successful under the above conditions.
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-
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36
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0009624573
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I. Flemming, R. Henning and H. Plaut, J. Chem. Soc., Chem. Commun., 1984, 29.
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J. Chem. Soc., Chem. Commun.
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Flemming, I.1
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37
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33748733680
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note
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4N·F were 84, 0 and 0% respectively.
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-
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38
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0000485694
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K. Tamao, N. Ishida and M. Kumada, J. Org. Chem., 1983, 48, 2120;
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Tamao, K.1
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Kumada, M.3
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