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Volumn 37, Issue 11, 1981, Pages 2091-2096

Oxidation of α,β-un saturated aldehydes

(3) Bal, Balkrishna S a Childers Jr , Wayne E a Pinnick, Harold W a

a UNIVERSITY OF GEORGIA (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33748664603 PISSN: 00404020 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4020(01)97963-3 Document Type: Article

Times cited : (1146)

References (30)

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5
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- Potassium permanganate oxidizes both aliphatic and aromatic aldehydes to acids but also will attack the double bond of α,β-unsaturated acids
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6
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10
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11
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19
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- Morton¹

20
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- Another hindered aldehyde (ii) can be oxidized to the corresponding methyl ester in 80% crude yield. This is the only example known to the authors of successful oxidation of a hindered aldehyde by this method. We thank Dr. Armand B. Pepperman for details of this conversion.

21
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- 194. A synthesis of vitamin a from cyclohexanone
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22
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- The free alcohol 1 (RH) forms an unidentified compound when allowed to react With TMSCN.

23
- 84918093044
- We thank Professor Wolfgang Kreiser for pointing out this method.

24
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- 1H NMR, IR and GC/MS data.

25
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- 1

26
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- Preparation of Carboxylic Acids from Aldehydes (Including Hydroxylated Benzaldehydes) by Oxidation with Chlorite.
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27
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28
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29
- 84918093041
- The amounts of E and Z isomers were determined by GC analysis on a QF-1/carbowax column. The acids were analyzed as the methyl esters. We thank Dr. Richard R. Hautala for determining these ratios.

30
- 84918093040
- We thank the Shell Chemical Company for a generous sample of “t-amylene”.

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