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A Renishaw μ-Raman 1000 system equipped with an X-Y stage and a CCD detector was used in this experiment. A He-Ne laser (λ = 632.8 nm) was employed as the excitation light source. An optical microscope was used to position the focused light beam onto the desired region of the sample surface. At present we are also trying to map the sample surface using this μ-Raman system; thus, we may directly compare it with an AFM image.
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