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1
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0003428791
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(a) See, for example, R. A. Moss, M. Jones, Wiley, New York
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(1975)
Carbenes
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Clos, G.L.1
Caspar, P.P.2
Hammond, G.S.3
Hartzler, H.D.4
Mackay, C.5
Seyferth, D.6
Trozollo, A.M.7
Wassermann, E.8
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12
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84989513691
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−1] = 1657(w), 1413(m), 1325(w), 1300(w), 1270(m), 1241 (m), 1171(m), 1116(m), 1073(m), 1058(w), 1009(m), 984(m), 967(s), 940(w), 924(w), 885(w), 867(m), 798(w), 784(m), 737(w), 655(w), 597(w), 581(m), 569(m), 525(w), 453(w), 423(w), 383(vs), 366(s), 349(m), 313(w), 228(w). Correct C,H analysis. NMR of the reaction mixture is essentially identical to that of the redissolved pure material.
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-
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13
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84989562804
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w = 0.0437 for 951 observed reflections with 1 > 3.00σ(I) and with 162 parameters. All calculations were performed on a VAX computer using the SHELX 76 crystallographic software package of Crystal Structure Determination, SHELX 76. Program for Crystal Structure Determination, University of Cambridge, Cambridge (UK) 1976.
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Sheldrick, G.M.1
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14
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84989540175
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(b) Further details of the crystal structure investigations are available on request from the Director of the Cambridge Crystallographic Data Centre, 12 Union Road, GB‐Cambridge CB2 1EZ (UK), on quoting the full journal citation.
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16
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84956108387
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Organylarsino-substituierte Schwefeldiimide: Die Kristallstrukturanalysen von 3, 7-Di-t-butyl-3H, 7H,-1?4, 5?4, 2, 4, 6, 8, 3, 7-dithiatetrazadiarsocin und Bis(diphenylarsino)schwefeldiimid
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(1984)
Z. Anorg. Allg. Chem.
, vol.513
, pp. 160
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Gieren, A.1
Betz, H.2
Hübner, T.3
Lamm, V.4
Herberhold, M.5
Guldner, K.6
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19
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84984363869
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Versuche zur Synthese von Heterocyclen mit Phosphor—Arsen- und Arsen—Arsen-Bindung: Reaktionen von Arsan-substituierten Cyan(triphenylphosphoranyliden)methanen mit Dichloraminophosphanen und -arsanen
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(1989)
Chemische Berichte
, vol.122
, pp. 1417
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Grützmacher, H.1
Pritzkow, H.2
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20
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84989536318
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w = 0.0587 for 814 observed reflections with 1 > 3.00σ(I) and with 73 parameters. All calculations were performed on a VAX computer using the TEXSAN crystallographic software package of Molecular Structure Corporation (TEXSAN‐TEXRAY Single Crystal Structure Analysis Package, Version 5.0, Molecular Structure Corporation, The Woodlands, Texas, 1989). See also [7b].
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21
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84989528790
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−1] = 1416(m), 1282(w), 1252(m), 1149(w), 1137(w), 941 (w), 932(w), 907(m), 831(m), 811(m), 668(w), 652(w), 597(w), 441(w), 429(w), 377(vs), 370(vs) correct C,H analysis.
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22
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84989528787
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w = 0.0583 for 2210 observed reflections with I > 3.00σ(I) and with 236 parameters. All calculations were performed on a VAX computer using the TEXSAN crystallographic software package of Molecular Structure Corporation (TEXSAN‐TEXRAY Structure Analysis Package, Molecular Structure Corporation, 1989). See also [7b].
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24
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84982066903
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Über Arsen-haltige Heterocyclen, I. Molekül- und Kristallstruktur von 2-Chlor-1,3,6,2-trithiarsaocan
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(1974)
Chemische Berichte
, vol.107
, pp. 2601
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Dräger, M.1
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