Preparation of solanesol from a tobacco leaf extract using high speed countercurrent chromatography

Journal of Liquid Chromatography and Related Technologies

Volumn 29, Issue 17, 2006, Pages 2587-2592

  Du, Qizhen ^a   Daijie, Wang ^a   Ito, Yoichiro ^b  

^a ZHEJIANG GONGSHANG UNIVERSITY   (China)

^b NATIONAL HEART LUNG AND BLOOD INSTITUTE   (United States)

Author keywords

High speed countercurrent chromatography; Separation; Solanesol; Tobacco leaves

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; ETHANOL; EXTRACTION; METHANOL; SEPARATION;

HIGH SPEED COUNTERCURRENT CHROMATOGRAPHY; SOLANESOL; TOBACCO LEAVES;

TOBACCO;

ALCOHOL; HERBACEOUS AGENT; METHANOL; PETROLEUM ETHER; PLANT EXTRACT; SOLANESOL; UNCLASSIFIED DRUG;

ARTICLE; COUNTER CURRENT CHROMATOGRAPHY; DRUG ISOLATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PLANT LEAF; TOBACCO;

CHROMATOGRAPHY; ETHANOL; EXTRACTION; METHANOL; SEPARATION; TOBACCO;

NICOTIANA TABACUM;

EID: 33748503648     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070600915197     Document Type: Article

References (12)

1. Rowland, R.L.; Latimer, P.H.; Giles, J.A. Flue-cured tobacco. I. Isolation of solanesol, an unsaturated alcohol. J. Am. Chem. Soc. 1956, 78, 4680-4683.
2. Morton, R.A. The chemistry and biochemistry of polyprenyl alcohols such as solanesol and dolichol. Biochem. J. 1972, 128 (1), 11.
3. Erickson, R.E.; Shunk, C.H.; Trenner, N.R.; Arison, B.H. Coenzyme Q. XI. The structure of solanesol. J. Am. Chem. Soc. 1959, 81, 4999-5001.
4. Serebryakov, E.P.; Nigmatov, A.G. Biologically active derivatives of polyprenylacetic acids and related compounds (review). Pharma. Chem. J. 1990, 24, 88-98.
5. Khidyrova, N.K.; Shakhidoyatov, K.M. Plant polyprenols and their biological activity. Chem. Nat. Comp. 2002, 38, 107-121.
6. Keca, M.; Gross, S.; Malnar, I. Isolation of solanesol from tobacco Nicotiana tabacum L.) by classic extraction and ultrasound extraction. Farm. Glas. 1997, 53, 173-182.
7. Xia, W.; Yu, D.-H.; Chen, X.-Z. Isolation of solanesol from discarded tobacco extracts. Chinese J. Pharma. 2003, 34, 328-329.
8. Du, Q.-Z.; Shu, A.; Ito, Y. Purification of fish oil ethyl esters by high speed countercurrent chromatography using non-aqueous solvent systems. J. Liq. Chromatogr. 1996, 19, 1451-1457.
9. Zhou, Y.; Chen, F.; Li, Z. Preparative separation of β-sitosterol by high speed countercurrent chromatography. J. Liq. Chromatogr. & Rel. Technol. 2002, 25, 1693-1701.
10. Woolen, B.H.; Jones, D.H. A rapid method for the estimation of solanesol by thin-layer densitometry. J. Chromatogr. 1971, 61, 180-182.
11. Zhao, J.; Wang, C.; Sun, X. Determination of solanesol in the extracts of tobacco leaves by high performance liquid chromatography. Chinese J. Chromatogr. 1997, 15 (6), 544-547.
12. 13C magic angle spinning NMR. J. Agric. Food Chem. 1985, 33, 419-425.