Syntheses, properties and Mössbauer studies of mono- and di-nitrile phosphine complexes of iron(II). Crystal structures of trans-[Fe(NCR)2(Et2PCH2CH2PEt 2)2][BF4]2 (R = Me or CH2C6H4OMe-4)

Journal of the Chemical Society - Dalton Transactions

Volumn , Issue 19, 1998, Pages 3311-3317

  Martins, Luísa M D R S ^a   Duarte, M Teresa ^a   Galvão, Adelino M ^a   Resende, Catarina ^a   Pombeiro, Armando J L ^a   Henderson, Richard A ^b   Evans, David J ^b  

^a INSTITUTO SUPERIOR TÉCNICO   (Portugal)

^b JOHN INNES CENTRE   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33748483847     PISSN: 03009246     EISSN: None     Source Type: Journal    
DOI: 10.1039/a804193h     Document Type: Article

References (36)

1. See, e.g. R. R. Eady, Adv. Inorg. Chem., 1991, 36, 77.
2. (a) D. L. Hughes, G. J. Leigh, M. Jimenez-Tenorio and A. T. Rowley, J. Chem. Soc., Dalton Trans., 1993, 75;
3. (b) A. Hills, D. L. Hughes, M. Jimenez-Tenorio and G. J. Leigh, J. Chem. Soc., Dalton Trans., 1993, 3041;
4. (c) G. J. Leigh and M. Jimenez-Tenorio, J. Am. Chem. Soc., 1991, 113, 5862.
5. M. A. N. D. A. Lemos and A. J. L. Pombeiro, J. Organomet. Chem., 1987, 332, C17.
6. D. L. Hughes, M. Jimenez-Tenorio, G. J. Leigh and A. T. Rowley, J. Chem. Soc., Dalton Trans., 1993, 3151.
7. A. Hills, D. L. Hughes, M. Jimenez-Tenorio, G. J. Leigh, C. A. McGeary, A. T. Rowley, M. Bravo, C. E. McKenna and M.-C. McKenna, J. Chem. Soc., Chem. Commun., 1991, 522.
8. D. J. Evans, M. Jimenez-Tenorio and G. J. Leigh, J. Chem. Soc., Dalton Trans., 1991, 1785.
9. J. E. Barclay, G. J. Leigh, A. Houlton and J. Silver, J. Chem. Soc., Dalton Trans., 1988, 2865.
10. J. Silver, Inorg. Chim. Acta, 1991, 184, 235.
11. R. V. D. Parish and B. E. Riley, J. Chem. Soc., Dalton Trans., 1979, 482.
12. G. M. Bancroft, Coord. Chem. Rev., 1973, 11, 247 and refs. therein.
13. (a) J. M. Bellerby and M. J. Mays, J. Chem. Soc., Dalton Trans., 1975, 1281;
14. (b) G. M. Bancroft, R. E. B. Garrod, A. G. Maddock, M. J. Mays and B. E. Prater, J. Am. Chem. Soc., 1972, 94, 647;
15. (c) G. M. Bancroft, M. J. Mays, B. E. Prater and F. P. Stefanini, J. Chem. Soc. A, 1970, 2146.
16. L. M. D. R. S. Martins, A. J. L. Pombeiro and R. A. Henderson, Inorg. Chim. Acta, 1996, 250, 311.
17. K. F. Purcell and R. S. Drago, J. Am. Chem. Soc., 1966, 88, 919.
18. N. B. Colthup, L. H. Daly and S. E. Wiberley, Introduction to Infrared and Raman Spectroscopy, Academic Press, New York, 1964.
19. M. F. C. Guedes da Silva, J. J. R. Fraústo da Silva and A. J. L. Pombeiro, J. Organomet. Chem., 1996, 526, 237;
20. M. F. C. Guedes da Silva, PhD Thesis, Instituto Superior Técnico, 1993.
21. A. J. L. Pombeiro and R. L. Richards, J. Organomet. Chem., 1979, 179, 459.
22. G. M. Bancroft, M. J. Mays and B. E. Prater, J. Chem. Soc. A, 1970, 956.
23. R. V. Parish, NMR, NQR, EPR and Mössbauer Spectroscopy in Inorganic Chemistry, Ellis Horwood, New York, 1990, ch. 4.
24. L. M. D. R. S. Martins, M. F. C. Guedes da Silva, J. J. R. Fraústo da Silva and A. J. L. Pombeiro, Rapid Commun. Mass Spectrom., 1996, 10, 447.
25. M. I. Bruce and M. J. Liddell, Appl. Organomet. Chem., 1987, 1, 191.
26. A. R. Barron, G. Wilkinson, M. Motevalli and M. B. Hursthouse, Polyhedron, 1987, 6, 1089.
27. J. E. Barclay, D. J. Evans, D. L. Hughes and G. J. Leigh, J. Chem. Soc., Dalton Trans., 1993, 69.
28. J. E. Barclay, A. Hills, D. L. Hughes and G. J. Leigh, J. Chem. Soc., Dalton Trans., 1988, 2871.
29. C. Redshaw, G. Wilkinson, B. Hussain-Bates and M. B. Hursthouse, Polyhedron, 1993, 12, 363.
30. A. F. Williams, Acta Crystallogr., Sect. C, 1988, 44, 1895.
31. D. J. Evans, R. A. Henderson, A. Hills, D. L. Hughes and K. E. Oglieve, J. Chem. Soc., Dalton Trans., 1992, 1259.
32. T. Al Salih, M. T. Duarte, J. J. R. Frausto da Silva, A. M. Galvão, M. F. C. Guedes da Silva, P. B. Hitchcock, D. L. Hughes, C. J. Pickett, A. J. L. Pombeiro and R. L. Richards, J. Chem. Soc., Dalton Trans., 1993, 3015.
33. G. M. Sheldrick, SHELXS 86, Crystallographic Calculation Program, University of Cambridge, 1986.
34. G. M. Sheldrick, SHELXL 93, Crystallographic Calculation Program, University of Göttingen, 1993.
35. C. K. Johnson, ORTEP II," Report ORNL-5138, Oak Ridge National Laboratory, Oak Ridge, TN, 1976.
36. International Tables for X-Ray Crystallography, Kynoch Press, Birmingham, 1974, vol. 4.