Synthesis and characterization of 1-azido-2-nitro-2-azapropane and 1-nitrotetrazolato-2-nitro-2-azapropane

Propellants, Explosives, Pyrotechnics

Volumn 31, Issue 4, 2006, Pages 263-268

  Boese, Roland ^a   Klapötke, Thomas M ^b   Mayer, Peter ^b   Verma, Vikas ^b  

^a UNIVERSITY OF DUISBURG ESSEN   (Germany)

^b UNIVERSITY OF MUNICH   (Germany)

Author keywords

ANAP; Azides; Explosives; Nitramines; Nitrotetrazole; NTNAP; X ray

Indexed keywords

CHEMICAL BONDS; HYDROLYSIS; NITROGEN COMPOUNDS; NUCLEAR MAGNETIC RESONANCE; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION;

ANAP; AZIDES; NITRAMINES; NITROTETRAZOLE; NTNAP;

EXPLOSIVES;

EID: 33748465507     PISSN: 07213115     EISSN: 15214087     Source Type: Journal    
DOI: 10.1002/prep.200600035     Document Type: Article

References (19)

1. W.-H. Walther, T. M. Klapötke, G. Holl, Physical Chemical Characterization and Explosive Properties of Hydrazine Azide, 29th Int. Annual Conference of ICT, Karlsruhe, Germany, June 30-July 3, 1998, p. 134/1.
2. T. M. Klapötke, B. Krumm, G. Holl, M. Kaiser, Synthesis, Characterization and Quantum Chemical Computations of Hexanitrohexaaza- Isowurtzitane, 30th Int. Annual Conference of ICT, Karlsruhe, Germany, June 29-July 2, 1999, p. 120/1.
3. T. Habereder, A. Hammerl, G. Holl, T. M. Klapötke, J. Knizek, P. Mayer, H. Nöth, Methylsubstituted Hyrdazinium Azide Derivatives, 31st Int. Annual Conference of ICT, Karlsruhe, Germany, June 27-30, 2000, p. 150/1.
4. T. M. Klapötke, K. Karaghiosoff, P. Mayer, A. Penger, J. M. Welch, Synthesis and Characterization of 1,4-Dimethyl-5-Aminotetrazolium 5-Nitrotetrazolate, Propellants, Explos., Pyrotech. 2006, 31, 188.
5. 6. Propellants, Explos., Pyrotech. 2002, 27(1). 1.
6. G. Holl, T. M. Klapötke, K. Polborn, C. Rienäcker, Structure and Bonding in 2-Diazo-4,6-dinitrophenol (DDNP), Propellants, Explos., Pyrotech. 2003, 28, 153.
7. K. Karaghiosoff, T. M. Klapötke, A. Michailovski, H. Nöth, M. Suter. 1,4-Diformyl-2,3,5,6-tetranitropiperazine: a new primary explosive based on glyoxal. Propellants, Explos., Pyrotech. 2003, 28(1), 1.
8. T. M. Klapötke, B. Krumm, H. Piotrowski, K. Polborn, G. Holl, Synthesis and Structures of Trifluormethyl, Fluoro, and Azido Substituted Hexabenzyl-hexaazaisowurtzitanes and Isolation of a Novel Hexaazaisowurtzitane Based Polycycle, Chemistry - Eur. J., 2003, 0(9), 687.
9. 7, Propellants, Explos., Pyrotech. 2003, 28(4), 165.
10. S. Berger, K. Karaghiosoff, T. M. Klapötke, P. Mayer, H. Piotrowski, K. Polborn, R. L. Willer, J. J. Weigand, N-Nitroso and N-Nitraminotetrazoles, J. Org. Chem. 2006, 71(4), 1295.
11. J. Geith, G. Holl, T. M. Klapötke, J. J. Weigand, Mononitrobiuret (MNB) and 1,5-Dinitrobiuret (DNB): Pyrolysis Experiments and Thermochemistry. Combust. Flame 2004, 139, 358.
12. 3), Propellants, Explos., Pyrotech. 2004, 29, 3.
13. R. Boese, M. Nussbaumer, In Situ Crystallisation Techniques, in: Organic Crystal Chemistry. D. W. Jones (Ed.), Oxford University Press, Oxford, 1994, 20.
14. G. M. Sheldrick, SHELXL-97, Program for Crystal Structure Refinement, Universität Göttingen. 1997.
15. J. Denkstein, V. Kaderabek, Nitramines, I. N-Acetoxymethylnitramines, Collect. Czech. Chem. Commun. 1960, 25, 2334.
16. G. A. Gareev, L. P. Kirillova, V. M. Shul'gina, S. R. Buzilova, L. P. Vologdina, L. I. Vereshchagin, Reaction of some derivatives of 2-nitro-2-azapropanol with azoles, Zh. Org. Khim. 1988, 24(10), 2221.
17. E. F. Witucki, M. B. Frankel, Synthesis of novel energetic aliphatic compounds, J. Chem. Eng. Data, 1979, 24(3), 247.
18. T. M. Klapötke, C. M. Rienäcker, Drophammer Test Investigations on Some Inorganic and Organic Azides. Propellants. Explos., Pyrotech. 2001, 26, 43.
19. Reichel & Partner GmbH, http://www.reichel-partner.de/.