Refinement of the crystal structure of μ3-chloro- μ3-hydroxo-tris(μ-chloro)- tris[tetramethylethylenediaminenickel(II)] chloride, {[Ni(C6H 16N2)]3Cl4OH}Cl

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 220, Issue 2, 2005, Pages 226-228

  Miyamoto, K ^a   Koizumi, R ^b   Horn, E ^b   Fukuda, Y ^a  

^a OCHANOMIZU UNIVERSITY   (Japan)

^b RIKKYO UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33748353634     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (12)

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3. Hughes, D. L.; Larkworthy, L. F.; Leigh, G. J.; McGarry, C. J.; Sanders, J. R.; Smith, G. W.; de Souza, J. S.: Trinuclear Species in Vanadium(II) Chemistry. J. Chem. Soc., Chem. Commun. (1994) 2137-2138.
4. 4](tmeda = N,N,N′,N′- tetramethylethylenediamine): a VII-VIII Mixed Valence Complex. J. Chem. Soc., Chem. Commun. (1990) 951-953.
5. Edema, J. J. H.; Duchateau, R.; Gambarotta, S.; Bensimon, C.: Labile triangulo-Trititanium(II) and -Trivanadium(II) Clusters. Inorg. Chem. 30 (1991) 3585-3587.
6. Miyamoto, K.; Sakamoto, M.; Tanaka, C.; Horn, E.; Fukuda, Y.: Syntheses, Structures, Spectroscopic Properties and Thermal Behavior of Ni(II) Mixed Ligand Complexes with N,N,N′,N′-Tetramethylethylene-diamine, Benzoylacetonate and Halide Anion. Bull. Chem. Soc. Jpn., in press (2005).
7. Handley, D. A.; Hitchcock, P. B.; Leigh, G. J.: Triangulopentahalo- trimetal complexes of nickel(II) and cobalt(II) with N,N,N′,N′-N- tetramethylethane-1,2-diamine and related compounds. Inorg. Chim. Acta 314 (2001) 1-13.
8. Johnson, C. K.: ORTEP-II. A Fortran Thermal-Ellipsoid Plot Program. Report ORNL-5138, Oak Ridge National Laboratory, Tennessee, USA 1976.
9. 3-hydroxo-tris(N,N,N′N′- tetramethylethylenediamine)trinickel(II) Chloride. Finn. Chem. Lett. (1976) 6-11.
10. Turpeinen, U.: Studies on the crystal structures of nickel(II) complexes with N,N,N′,N′-tetramethylethylenediamine. Ann. Acad. Sci. Fenn. A2 (1977) 6-27.
11. Altomare, A.; Cascarano, G.; Giacovazzo, C.; Guagliardi, A.; Burla, M. C.; Polidori, G.; Camalli, M.: SIR92 - a program for automatic solution of crystal structures by direct methods. J. Appl. Crystallogr. 27 (1994) 435.
12. Molecular Structure Corporation: teXsan. Single Crystal Structure Analysis Software. Version 1.7. MSC, The Woodlands, Texas, USA 1995.