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33748274896
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note
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2O for La, Pr, and Yb by elemental analysis.
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28
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33748252261
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note
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3. 8539 reflections measured, 8503 unique used in all calculations. Final R1 = 0.0486. CCDC 265610 contains the supplementary crystallographic data for this paper.
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30
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0000085077
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The δ and φ angles/deg: δO2[O3O8]O4, 26.6; δO2[O1O8]O4, 24.8; δO6[O3O7]O4, 36.5_δO6[O1O7]O5, 15.6; φO6-O7-O8-O2, 8.1; φO1-O5-O4-O3, 0.3 as compared with 29.5°; 29.5°; 29.5°; 29.5°; 0.0°; 0.0° for the regular DD (Drew, M. G. B. Coord. Chem. Rev. 1977, 24, 179), respectively.
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Drew, M.G.B.1
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