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33748248829
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note
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Using a "seed" obtained after the thermal experiments of BPBN facilitated the preferential recrystallization of the β-phase.
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15
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33748283948
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note
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2) (all data) = 0.1001 for 4141 unique reflections. We found an anomaly of the residual electron density in the differential Fourier map and assumed the presence of a small portion of an isomeric and diamagnetic 3-tert-butylamino-5- phenyl-1,4-quinone-1-tert-butyliminoxide as a lattice defect. We applied a disorder model at the relating O and H atoms, and their occupancy parameter was included in the refinement. The purity of β-BPBN was determined to be 94.4%, being consistent with the magnetic measurements within an experimental error. The minor impurity might be formed via a thermal disproportionation process giving quinone imine N-oxides and N-tert-butylanilines.
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0029857173
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Fujita, J.1
Tanaka, M.2
Suemune, H.3
Koga, N.4
Matsuda, K.5
Iwamura, H.6
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2942732219
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Fujita, J.; Matsuoka, Y.; Matsuo. K.; Tanaka, M.; Akita, T.: Koga, N.; Iwamura, H. Chem. Commun. 1997, 2393.
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Fujita, J.1
Matsuoka, Y.2
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Akita, T.5
Koga, N.6
Iwamura, H.7
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19
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33748278737
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note
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-1 in DSC measurements.
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21
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37049127499
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Calder, A.; Forrester, A. R.: Hepburn, S. P. J. Chem. Soc., Parkin Trans. 1 1973, 456.
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(1973)
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Calder, A.1
Forrester, A.R.2
Hepburn, S.P.3
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22
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33748278199
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note
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-1 from 70 to 80 °C.
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23
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33748281967
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note
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A laser beam was introduced into a Quantum Design MPMS-7 SQUID probe through a quartz optical fiber. The light source was a CrystalLaser GCL-150-M (532 nm; diode-pumped green laser). The quartz fiber was purchased from Fujikura (large-core fiber S.800/1000; core diameter 800 μm). The polycrystalline specimen of α-BPBN was stuck on a small piece of a polyimide Kapton tape (duPont). The precise mass of BPBN was estimated from the magnetic susceptibility.
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