Modem thin-layer chromatography in pharmaceutical and drug analysis

Pharmacopeial Forum

Volumn 27, Issue 6, 2001, Pages 3420-3428

  Sherma, Joseph ^a  

^a LAFAYETTE COLLEGE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33747886678     PISSN: 03634655     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (67)

1. Sherma, J. Comparison of Thin Layer Chromatography and Liquid Chromatography. J. Assoc. Off. Anal. Chem.1991, 74,435437.
2. Fried, B; Sherma, J. Thin Layer Chromatography, 4th ed.; Marcel Dekker, Inc.: New York, NY, 1999.
3. Renger, B. Contemporary Thin Layer Chromatography in Pharmaceutical Analysis. J. AOAC Int. 1998, 81, 333-339.
4. "4. Kenyon, A.S.; Zuzack, J.; Patel, R.; and Le, V. Cost-Sparing Analyses Using a Rapid-Scanning Thin-Layer Chromatographie Method. PF24(4), 1998, 6607-6612.
5. USP 24-NF /P.The United States Pharmacopeial Convention, Inc.: Rockville, MD, 1999.
6. (201) Thin-Layer Chromatographie Identification Test. USP 24; United States Pharmacopeial Convention, Inc.: Rockville, MD, 1999;pl856.
7. (621) Chromatography. USP 24; United States Pharmacopeial Convention, Inc.: Rockville, MD, 1999; pp 1914-1926.
8. Thin-Layer Chromatography, Section 2.2.27. European Pharmacopoeia, 3rd ed., Supplement 2007;Council of Europe: Strasbourg; pp 10-11.
9. Ferenczi-Fpdor, K.; Vegh, Z.; Nagy-Turak, A.; Renger, B.; Zeller, M. Validation and Quality Assurance of Planar Chromatographie Procedures in Pharmaceutical Analysis. J. AOAC Int. 2001, 84, in press.
10. Habel, D; Guermouche, S.; and Guermouche, M.H. HPTLC Determination of Isoniazid and Acetylisoniazid in Serum. J. Planar Chromatogr.-Mod. TLC. 1997, 10, 453-156.
11. Popa, D.S.; Oprean, R.; Curea, E.; Preda, N. TLC-UV Densitometric and GC-MSD Methods for Simultaneous Quantification of Morphine and Codeine in Poppy Capsules. J. Pharm. Biomed. Anal. 1998, 18, 645-650.
12. Sherma, J; Incarvito, C.D. Analysis of Tablets and Caplets Containing Ketoprofen by Normal- and Reversed-Phase HPTLC with Ultraviolet Absorption Densitometry on Preadsorbent Plates. Acta Chromatogr. 1997, 7, 124-128.
13. Simonovska, B.; Prosek, M.; Vovk, I.; Jelen-Zmitek, A. High Performance Thin Layer Chromatographie Separation of Rantidine Hydrochloride and Two Related Compounds. J. Chromatogr. B. 1998, 715, 425-430.
14. Dhanesar, S.C. Quantitation of Antibiotics by Densitometry on a Hydrocarbon-Impregnated Silica Gel HPTLC Plate. Part IV: Quantitation and Evaluation Penicillins. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 180-185.
15. Lazaric, K.; Cucek, B.; Faust, G. RPTLC Method for Determining Parabins in Oral Antacid Suspension During Stability Testing. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 86-88.
16. Radembino, N.; Lofsau, P.M.; Dessalles, M.C.; Marchât, L.; Bories, C.; Gayral, P.; Mahuzier, G. Epoxyethane-/ethynesulfonamides with Antifilarial Activities. Arzneim. Forsch/Dnig Res. 1998, 48, 294-299.
17. Zaidi, F.; Voirn, B.; Jay, M.; Viricel, M.R. Free Flavonoid Aglycones from Leaves of Mentha pulegiiim and M. suaveolens (Labiatae). Phytochemistry. 1998, 48, 991-994.
18. Fater, Z.; Tasi, G.; Szabady, B.; Nyiredy, S. Identification of Amphetamine Derivatives by Uni-Dimensional Multiple Development and Two-Dimensional HPTLC Combined with Postchromatographic Derivatization. J. Planar Chromatogr.-Mod. TLC. 1998, //, 225-229.
19. Dong, C.; Xie, H.; Shuang, S.; Liu, C. Determination of Tetracycline and 4-Epimeric Tetracycline by TLC-Fluorescence Scanning Densitometry. Anal. Lett. 1999, 32, 1121-1130.
20. Darula, Z.; Torok, G.; Wettmann, G.; Mannekens, E.; Iterbeke, K.; Toth, G.; Tourwe, A.A. Rapid, Qualitative Thin Layer Chromatographie Method for the Separation of the Enantiomers of Unusual Aromatic Amino Acids. J. Planar Chromatogr.-Mod. TLC. 1998,11, 346-349.
21. Bhushan, R. ; Thuku, G.T. Direct Enantiomeric Resolution of Some 2-Arylpropionic Acids Using (-)-Brucine-Impregnated Thin Layer Chromatography. Biomed. Chromatogr. 1999, 13, 276-278.
22. Suedee, R.; Saelim, J.; Thavornpibulbut, T.; Srichana, T. Chiral Determination of Various Adrenergic Drugs by Thin Layer Chromatography Using Molecularly Imprinted Chiral Stationary Phases Prepared with alpha-Agonists. Analyst (Cambridge, U.K.). 1999,124, 1003-1009.
23. LeFevre, J.W.; Rogers, E.D.; Pico, L.L.; Bolting, C.L. The Effect of Structure on the Resolution of Dansyl Amino Acids Using beta-Cyclodextrin as a Mobile Phase Additive in Reversed Phase Thin Layer Chromatography. Chromatographia. 2000, 52, 648-652.
24. Szepesi, G.; Nyiredy, S. Pharmaceuticals and Drugs. In Handbook of Thin Layer Chromatography, 2nd ed.; Sherma, J., Fried, B., Eds.; Marcel Dekker, Inc.: New York, NY 1996; pp. 819-876.
25. Ng, L.L. Pharmaceuticals and Drugs. In Handbook of Thin Layer Chromatography; Sherma, J., Fried, B., Eds.; Marcel Dekker, Inc.: New York, 1991; pp. 717-755.
26. Romano, G.; Caruso, G.; Musumarra, G.; Pavone, p.; Cruciani, G. Qualitative Organic Analysis. Part 3. Identification of Drugs and their Metabolites by Standardized TLC Data. J. Planar Chromatogr.-Mod. TLC. 1994, 7, 233-241.
27. Ojanpera, I.; Ojansivu, R. L.; Nokua, J.; Vuori, E. Comprehensive TLC Drug Screening in Forensic Toxicology: Comparison of Findings in Urine and Liver. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 38-45.
28. Misztal, G. Thin Layer Reversed Phase Ion Pair Chromatography of Some Cephalosporins. J. Liq. Chromatogr. & Relat. Technol. 1999,22, 1589-1598.
29. Muller, D.; Ebel, S. Two-Dimensional Thin Layer Chromatographie Separation of H,-Antihistamines. J. Planar Chromatogr.-Mod. TLC. 1997,10, 420-426.
30. Poole, C.F. Planar Chromatography at the Turn of the Century. J. Chromatogr. A. 1999, 856, 399-427.
31. Kiss, B.D.; Mincsovics, E.; Nemes, K.B.; Klebovich, I. Application of OPLC-DAR and HPLC-RD Techniques in Metabolite Research. J. Planar Chromatogr.-Mod. TLC. 2000, 13, 257260.
32. Ojanpera, I.; Goebel, K.; Vuori, E. Toxicological Drug Screening by Overpressured Layer Chromatography. J. Liq. Chromatogr. & Relat. Technol. 1999, 22, 161-171.
33. Kassai, A.; Szecsi, A.; Koppany, A.; Vegh, Z.; FerencziFodor, K. Analytical Transfer of an OPLC Purity Test and Its Application for In-Process Monitoring. J. Planar Chromatogr.-Mod. TLC. 2000, 13, 30-32.
34. Vilceanu, N.; Nitescu, I. Purity Evaluation Study of Methyldopa Lot I USP-Standard Substances. Note II. Methyldopa TLC Purity Testing. Farmacia(Bucharest). 2000, 48, 37-44.
35. DiGregorio, D.; Sherma, J. Analysis of the Active Ingredient Magnesium Salicylate in Analgesic Tablets by HPTLC with Ultraviolet Absorption Densitometry. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 230-232.
36. Wang, P.; Zhou, M.; Feng, Y; Chen, L. Simultaneous Determination of Trace Ofloxacin and Enoxacin by TLC-Fluorescence Spectrodensitometry. Anal. Lett. 1998, 31, 1523-1531.
37. Hostettmann, K.; Terreaux, C.; Marston, A.; Porterai, O. The Role of Planar Chromatography in the Screening and Isolation of Bioactive Compounds from Medicinal Plants. J. Planar Chromatogr.-Mod. TLC. 1997,10, 251-257.
38. Zweig, G.; Sherma, J., Handbook of Chromatography; CRC Press: Boca Raton, FL, 1972; Vol. II, pp 103-189.
39. Jork, H.; Funk, W.; Fischer, W.; Wimmer, H. Thin Layer Chromatography, Reagents and DeteclionMethods, Physical and Chemical Detection Methods Fundamentals, Reagents I; VCH: Weinheim, Germany, 1990; vol. la.
40. Jork, H.; Funk, W.; Fischer, W.; Wimmer, H. Thin Layer Chromatography, Reagents and Detection Methods, Physical and Chemical Detection Methods: Activation Reactions, Reagent Ser' ies. Reagents H; VCH: Weinheim, Germany, 1993; vol Ib.
41. Hahn-Deinstrop, E.; Koch, A.; Mueller, M. Guidelines for the Assessment of the Traditional Herbal Medicine "Olibanum" by Application of HPTLC arid Desaga ProViDoc Video Documentation. J. Planar Chromatogr.-Mod. TLC. 1998, 11, 404-410.
42. Rozylo, J.K.; Siembida, R.; Jamrozek-Manko, A. A New Simple Method for Documentation of TLC Plates. J. Planar Chromatogr.-Mod. TLC. 1997,10, 225-228.
43. Stahlmann, S.A. Ten-Year Report on HPTLC-FTIR Online Coupling. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 5-12.
44. Wilson, I.D.; Spraul, M.; Humpfer, E. Thin Layer Chromatography Combined with High Resolution Solid State NMR for Compound Identification without Substance Elution: Preliminary Results. J. Planar Chromatogr.-Mod. TLC. 1997,10,217-219.
45. Brzezinka, H.; Dallakian, P.; Budzikiewicz, H. Thin Layer Chromatography and Mass Spectrometry for Screening of Biological Samples for Drugs and Metabolites. J. Planar Chromatogr.Mod. TLC. 1999, 12, 96-108.
46. Kenyon, A.S.; Xiaoye, S.; Van, W; Ng, W.H.; Prestridge, R.; Sharp, K. Simple, At-Site Detection of Diethylene Glycol/Ethylene Glycol Contamination of Glycerin and Glycerin-Based Raw Materials by Thin Layer Chromatography. J.AOACInt. 1998, 81, 44-50.
47. Fu, Q.; He, L.; Miao, Z. Analysis of Strychnine Alkaloids in Biological Samples by Thin Layer Chromatographie Densitometry and Distribution Study of Strychnine in Intoxicated Rats. J. Xi'anMed. 1998, 10, 146-149.
48. Hahn-Dienstrop, E. Applied Thin Layer ChromatographyBest Practice and Avoidance of Mistakes; Wiley-VCH Verlag GmbH: Weinheim, Germany, 2000.
49. Essig, S.; Kovar, K.A. Impurity Test of Theophylline: Comparison of Classical Slit Scanner with Videodensitometry. J. Planar Chromatogr.-Mod. TLC, 1999, 12, 63-65.
50. Petrovic, M.; Kastelan-Macan, M.; Babic, S. Quantitative Evaluation of 2D Chromatograms with a CCD Camera. J. Planar Chromatogr.-Mod. TLC. 1998, 11, 353-356.
51. Sherma, J. A Field Guide to Instrumentation: Quantitative Thin Layer Chromatography Densitometers. Inside Laboratory Management. 2000, 4 (10),.-12-18.
52. Szepesi, G. Somè Aspects of the Validation of Planar Chromatographie Methods in Pharmaceutical Analysis. I: General Principles and Practical Approaches. J. Planar Chromatogr.-Mod. TLC. 1993,6, 187-197.
53. Szepesi, G. Some Aspects of the Validation of Planar Chromatographie Methods Used in Pharmaceutical Analysis. II. Ruggedness Testing. J. Planar Chromatogr.-Mod. TLC. 1993, 6, 259-268.
54. Vovk, I.; Golc-Wondra, A.; Prosek, M. Validation of an HPTLC Method for Caffeine. J. Planar Chromatogr.-Mod. TLC. 1997,70,416-419.
55. Ferenczi-Fodor, K.; Nagy-Turak, A.; Vegh, Z. Validation and Monitoring of Quantitative Thin Layer Chromatographie Purity Tests for Bulk Drug Substances. J. Planar Chromatogr.-Mod. TLC. 1995, 8, 349-356.
56. CPMP Working Party On Quality of Medicinal Products: Tripartite ICH Text: Validation of Analytical Procedures, Draft No. 3 (III/5626/93-EN) Bruxels, September 1993.
57. Note for Guidance: Validation of Analytical Procedures, Final, Committee for Proprietary Medicinal Products, Document No. III/5626/94-EN, Bruxels, 1994.
58. Renger, B.; Jehle, H.; Fischer, M.; Funk, W. Validation of Analytical Procedures in Pharmaceutical Analytical Chemistry: HPTLC Assay of Theophylline in an Effervescent Tablet. J. Planar Chromatogr.-Mod. TLC. 1995, 8, 269-278.
59. ICH Guidelines Q2A, Validation of Analytical Procedures: Definition and Terminology (CPMP 111/5626/94), Geneva, Switzerland, March 1995.
60. ICH Guideline Q2B, Validation of Analytical Procedures: Methodology (CPMP/ICH/281/95), Geneva, Switzerland, November 1996.
61. Renger, B. Benchmarking of HPLC and HPTLC in Pharmaceutical Analysis. J. Planar Chromatogr.-Mod. TLC. 1999, 12, 58-62.
62. Renger, B. Quantitative Planar Chromatography as a Tool in Pharmaceutical Analysis. J. AOAC Int. 1993, 76, 7-13.
63. Kulkarni, S.P.; Amin, P.D. Stability Indicating HPTLC Determination of Timolol Maleate as Bulk Drug and in Pharmaceutical Preparations. J. Pharm. Biomed. Anal. 2000,23, 983-987.
64. Koh, D.; Tan, C.; Ng, S.K.; Tan, B.T.; Leow, Y.H.; Goh, C.L. Screening forp-Phenylenediamine (PPD) in Hair-Care Products by TLC. Contact Dermatitis. 2000, 43, 182-183.
65. Xie, P.; Van, Y.; Qian, H.; Lin, Q. Fluorophptometric TLC Assay of Ginko Terpenes by Ppst-Chromatographic Thermochemical Derivatization and Quality Survey of Commercial Ginko Products. J. AOAC Int. 2001, 84, in press.
66. Sherma, J. Planar Chromatography. Anal. Chem.2000, 72, in press. (Bienniel reviews of TLC have been published each evennumbered year in the review issue of Anal. Chem. since 1970).
67. Sherma, J; Fried, B. Handbook of Thin Layer Chromatography, 2nd ed.; Marcel Dekker, Inc.,: New York, NY, 1996.