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Volumn 47, Issue 39, 2006, Pages 7017-7019

Metal triflate catalyzed highly regio- and stereoselective 1,2-bromoazidation of alkenes using NBS and TMSN3 as the bromine and azide sources

Author keywords

, Unsaturated carbonyl compounds; Alkenes; anti 1,2 Bromoazides; Bromoazidation; Catalyst; Metal triflate; N Bromosuccinimide (NBS); Trimethylsilyl azide (TMSN3)

Indexed keywords

ALKENE; ALKENE DERIVATIVE; AZIDE; BROMINE; CARBONYL DERIVATIVE; METAL; N BROMOSUCCINIMIDE; TRIFLUOROMETHANESULFONIC ACID; TRIMETHYLSILYL DERIVATIVE;

EID: 33747807394     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.07.110     Document Type: Article
Times cited : (29)

References (23)
  • 3
    • 0001882768 scopus 로고
    • For the synthesis of tetrazoles via Hassner-Ritter reaction:
    • For the synthesis of tetrazoles via Hassner-Ritter reaction:. Ranganathan S., Ranganathan D., and Mehrotra A.K. Tetrahedron Lett. 14 (1973) 2265-2268
    • (1973) Tetrahedron Lett. , vol.14 , pp. 2265-2268
    • Ranganathan, S.1    Ranganathan, D.2    Mehrotra, A.K.3
  • 20
    • 33747762693 scopus 로고    scopus 로고
    • note
    • 4 and concentrated under vacuum. The bromoazide product was purified by flash column chromatography using petroleum ether-EtOAc as an eluent.
  • 21
    • 33747796023 scopus 로고    scopus 로고
    • note
    • 3): δ 25.9, 27.8, 50.3, 65.1, 126.6, 128.7, 129.1, 129.7, 130.5, 135.3.
  • 22
    • 33747803362 scopus 로고    scopus 로고
    • note
    • 4 and concentrated under vacuum. The bromoazide product was purified by flash column chromatography using petroleum ether-EtOAc as an eluent.
  • 23
    • 33747759453 scopus 로고    scopus 로고
    • note
    • 3): δ 46.0, 53.2, 55.1, 66.7, 114.1 (2C), 126.9, 129.1 (2C), 160.2, 168.5.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.