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Volumn 47, Issue 38, 2006, Pages 6821-6823

An efficient method for chlorination of alcohols using PPh3/Cl3CCONH2

Author keywords

Alcohols; Chlorination; Trichloroacetamide; Triphenylphosphine

Indexed keywords

ALCOHOL; ALCOHOL DERIVATIVE; CHLORIDE; CHLORINE DERIVATIVE; OCTANOL;

EID: 33747449011     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.07.060     Document Type: Article
Times cited : (37)

References (30)
  • 6
    • 0008320902 scopus 로고
    • Copenhaver J.E., and Whaley A.M. (Eds), Wiley and Sons, New York
    • In: Copenhaver J.E., and Whaley A.M. (Eds). Organic Syntheses Vol. 1 (1941), Wiley and Sons, New York 144-145
    • (1941) Organic Syntheses , vol.1 , pp. 144-145
  • 21
    • 33747407109 scopus 로고    scopus 로고
    • Chaysripongkul, S.; Pluempanupat, W.; Jang, D. O.; Chavasiri, W., submitted for publication.
  • 22
    • 33747446742 scopus 로고    scopus 로고
    • note
    • 2 ratio and reaction time.
  • 23
    • 33747423770 scopus 로고    scopus 로고
    • note
    • 3): δ 4.01 (sex, J = 6.5 Hz, 1H), 1.69 (m, 2H), 1.28-1.50 (m, 11H), 0.89 (t, J = 6.7 Hz, 3H).
  • 25
    • 33747422221 scopus 로고    scopus 로고
    • note
    • The stereochemistry was determined by comparison with S-(+)-2-octyl chloride by HPLC using commercially available chiral columns (column cyclobond I 2000).
  • 28
    • 33747397023 scopus 로고    scopus 로고
    • note
    • 3 (1.5 equiv) at rt (30 °C) or 40 °C, 1 h.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.