Preparative separation of saponins from the Luffa cylindeica (L.) Roem. by slow rotary countercurrent chromatography

Journal of Liquid Chromatography and Related Technologies

Volumn 29, Issue 16, 2006, Pages 2451-2456

  Du, Qizhen ^a   Gao, Shijun ^a  

^a ZHEJIANG GONGSHANG UNIVERSITY   (China)

Author keywords

Lucyoside H; Lucyoside Q; Luffa cyclindrica; Preparative isolation; Saponins; Slow rotary countercurrent chromatography

Indexed keywords

CHLOROFLUOROCARBONS; CHROMATOGRAPHY; EXTRACTION; METHANOL; SOLVENTS;

LUCYOSIDE H; LUCYOSIDE Q; LUFFA CYCLINDRICA; PREPARATIVE ISOLATION; SAPONINS; SLOW ROTARY COUNTERCURRENT CHROMATOGRAPHY;

METABOLITES;

CHLOROFORM; LUCYOSIDE H; LUCYOSIDE Q; LUFFA CYLINDEICA EXTRACT; METHANOL; SAPONIN DERIVATIVE; SOLVENT; UNCLASSIFIED DRUG; WATER;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COUNTER CURRENT CHROMATOGRAPHY; COUNTERCURRENT EXTRACTION; ELECTROSPRAY MASS SPECTROMETRY; LUFFA; LUFFA CYLINDEICA; NONHUMAN; PROTON NUCLEAR MAGNETIC RESONANCE; REACTION OPTIMIZATION; SEPARATION TECHNIQUE; SLOW ROTARY COUNTERCURRENT CHROMATOGRAPHY; STRUCTURE ANALYSIS;

CUCURBITA; LUFFA;

EID: 33747091926     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070600864924     Document Type: Article

References (11)

1. Jiangsu New Medicinal College, Dictionary of Chinese Herb Medicines; Shanghai Scientific Technologic Publisher: Shanghai, 1977.
2. He, G.; Liu, Y.; Qi, S. Some pharmacodynamic studies on Luffa saponin. West China J. Pharm. Sci. 1997, 12 (2), 76-78.
3. Liang, L.; Lu, L.; Cai, Y. Studies on the chemical components from leaves of Luffa cylinderica Roem. Acta Pharm. Sin. 1993, 28 (11), 38-41.
4. Liang, L.; Lu, L.; Cai, Y. Study on the chemical components from leaves of Luffa cylinderica Roem.(III). West China J. Pharm. Sci. 1994, 9 (4), 209-210.
5. Liang, L.; Lu, L.; Cai, Y.; Liu, C. Studies on the Chemical Components from Leaves of Luffa cylindrica. J. Chin. Med. Mat. 1995, 18 (8), 24-25.
6. Liang, L.; Liu, C.; Li, G.; Lu, L.; Cai, Y. Studies on the chemical components from leaves of Luffa cylindrica Roem. Acta Pharm Sin. 1996, 31 (2), 122-125.
7. Liang, L.; Liu, C.; Li,G.; Lu, L.; Cai, Y. Studies on the chemical structure of lucyoside R from leaves of Luffa cylindrica Roem. Acta Pharm. Sin. 1997, 32 (10), 42-45.
8. Takemoto, T.; Arihara, S.; Yoshikawa, K.; Yano, I.; Hayashi, T. Studies on the constituents of Cucurbitaceae plants VI. On the saponin constituents of Luffa cylindrica Roem.(1). Yakugaku Zasshi 1984, 104, 246-255.
9. Du, Q.; Wu, P.; Ito, Y. Low-speed rotary countercurrent chromatography using a convoluted multilayer helical tube for industrial separation. Anal. Chem. 2000, 72 (14), 3363-3365.
10. Du, Q.; Ito, Y. Low rotary countercurrent chromatography. J. Liq. Chromatogr. & Rel. Technol. 2003, 26, 1827-1838.
11. Du, Q.; Jerz, G.; He, Y.; Li, L.; Xu, Y.; Zhang, Q.; Zheng, Q.; Winterhalter, P.; Ito, Y. Semi-industrial isolation of salicin and amygdalin from plant extracts using slow rotary counter-current chromatography. J. Chromatogr. A 2005, 1074, 43-46.