Synthesis and analysis of a versatile imine for the undergraduate organic chemistry laboratory

Journal of Chemical Education

Volumn 83, Issue 8, 2006, Pages 1221-1224

  Bennett, Jacqueline ^a,b   Meldi, Kristen ^a   Kimmell II, Christopher ^a  

^a DRURY UNIVERSITY   (United States)

^b STATE UNIVERSITY OF NEW YORK   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMMONIA; CHEMICAL ANALYSIS; DISTILLATION; EXPERIMENTS; FILTRATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; PURIFICATION; SYNTHESIS (CHEMICAL);

IMINE; ORGANIC CHEMISTRY; VACUUM DISTILLATION; VACUUM FILTRATION;

CHEMISTRY;

EID: 33746943694     PISSN: 00219584     EISSN: None     Source Type: Journal    
DOI: 10.1021/ed083p1221     Document Type: Article

References (25)

1. (a) Manhas, M. S.; Ghosh, M.; Bose, K. J. Org. Chem. 1990, 55, 575-580.
2. (b) Taggi, A. E.; Hafez, A. M.; Lectka, T. Acc. Chem. Res. 2003, 36 10-19.
3. (c) Nishiwaki, N.; Knudsen, K. R.; Gothelf, K. V.; Jorgensen, K. A. Agnew. Chem., Int. Ed. Engl. 2001, 40, 2992-2995.
4. (a) Chowdari, N. S.; Ramachary, D. B.; Barbas, C. F. Synlett. 2003, 12, 1906-1909.
5. (b) Cordova, A. Acc. Chem. Res. 2004, 37, 102-112.
6. (c) Cordova, A.; Notz, W.; Zhong, G.; Betancort, J. M.; Barbas, C. F. J. Am. Chem. Soc. 2002, 124, 1842-1843.
7. (d) Cordova, A.; Watanabe, S.; Tanaka, F.; Notz, W; Barbas, C. F. J. Am. Chem. Soc. 2002, 124, 1866-1867.
8. (e) List, B. J. Am. Chem. Soc. 2000, 122, 9336-9337.
9. (a) Nelson, D. L.; Cox, M. M. Lehninger Principles of Biochemistry; Worth Pub.: NY, 2000.
10. (b) Campbell, M. K.; Farrell, S. O. Biochemistry; Brooks/Cole: Montery, CA, 2003.
11. (a) Jones, M. Organic Chemistry; W. W. Norton: New York, 1997.
12. (b) McMurry, J. Organic Chemistry, 6th ed.; Brooks/Cole: Montery, CA, 2004.
13. (c) Carey, F. A. Organic Chemistry 6th ed.; McGraw-Hill: New York, 2006.
14. (d) Hornback, J. M. Organic Chemistry, 2nd ed.; Thomson Brooks/Cole: London, 2006.
15. (a) Mohrig, J. R.; Hammond, C. N.; Morrill, T. C.; Schatz, P. F.; Morrill, T. C. Modern Projects and Experiments in Organic Chemistry: Miniscale and Standard Taper Microscale, 2nd ed.; W. H. Freeman: New York, 2003.
16. (b) Pavia, D. L.; Lampman, G. M.; Kriz, G. S.; Engel, R. G. Introduction to Organic Laboratory Techniques: A Small Scale Approach, 2nd ed.; Brooks/Cole: Montery, CA, 2005.
17. (c) Lehman, J. W. Operational Organic Chemistry: A Problem-Solving Approach to the Laboratory Course, 3rd ed.; Prentice Hall: Upper Saddle River, NJ, 1999.
18. (d) Williamson, K. L. Organic Experiments, 9th ed.; Houghton Mifflin: Boston, 2002.
19. (a) Todd, D. J. Chem. Educ. 1992, 69, 584.
20. (b) Sartori, A. T.; Wood, W. F. J. Chem. Educ. 1992, 69, 572.
21. (c) Amigoni, S.; Penverne, C.; Nugier-Chauvin, C.; Le Floc'h, Y. J. Chem. Educ. 1999, 76, 1247.
22. SDBS Home Page. http://www.aist.go.jp/RIODB/SDBS/menue.html (accessed Mar 2006).
23. Haddleton, D. M.; Crossman, M. C.; Dana, B. H.; Duncalf, D. J.; Heming, A. M.; Kukulj, D.; Shooter, A. J. Macromolecules 1999, 32, 2110-2119.
24. (a) Yeh, H. J. C.; Ziffer, H.; Jerina, D. M.; Boyd, D. R. J. Am. Chem. Soc. 1973, 95, 2741-2743.
25. (b) Bahmanyar, S.; Houk, K. N. Org. Lett. 2003, 5, 1249-1251.