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33746423425
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note
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2-) was determined by titration.
-
-
-
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28
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33746395008
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note
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4, and solvent evaporated under reduced pressure. The crude product was purified by column chromatography on silica gel to afford pure material.
-
-
-
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29
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33746397958
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note
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2 in a desiccator under vacuum for subsequent reaction.
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