Analytical method for the determination of chlorinated paraffins in environmental samples using GC-ECNI-ion trap-MS

Fresenius Environmental Bulletin

Volumn 15, Issue 6, 2006, Pages 571-577

  Přibylová, Petra ^a   Klánová, Jana ^a   Coelhan, Mehmet ^b   Holoubek, Ivan ^a  

^a MASARYK UNIVERSITY   (Czech Republic)

^b TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

Chlorinated paraffins (CPs); GC ECNI ion trap MS; Medium chain CPs (MCCPs); Polychlorinated n alkanes; Short chain CPs (SCCPs)

Indexed keywords

CHLORINATED HYDROCARBON; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; ORGANIC POLLUTANT; POLLUTION MONITORING;

CENTRAL EUROPE; CZECH REPUBLIC; EURASIA; EUROPE;

EID: 33746325161     PISSN: 10184619     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (15)

1. WHO (World Health Organization), Environmental Health Criteria 181: Chlorinated Paraffins., in WHO Geneva. 1996.
2. European Commission (1999) Alkanes, C10-13 Chloro, Short chain length chlorinated paraffins, Summary risk assessment report.
3. 13 Polychlorinated n-Alkanes in Canadian Midlatitude and Arctic Lake Sediments. Environ. Sci. Technol., 33, 2858-2863.
4. Chlorinated Paraffins Industry Association (2003) Chlorinated Paraffins Regulatory Update. October 2003. Washington D.C. http://www.regnet.com/cpia/ update1003.htm.
5. Gouvernment of the Czech Republic. (2003) Collection of laws. Ordinance No.61/2003.
6. Coelhan M. (1999) Determination of short-chain polychlorinated paraffins in fish samples by short-column GC/ECNI-MS. Anal. Chem., 71, 4498-4505.
7. Borgen, A.R., Schlabach, M. and Mariussen, E. (2003) Screening of chlorinated paraffins in Norway. Organohalogen Compd., 60, 331-334.
8. Huttig, J., Zencak, Z. and Oehme, M. (2004) Levels of chlorinated paraffins in North and Baltic sea sediments. Organohalogen Compd., 66, 1344-1349.
9. Reth, M. and Oehme, M. (2004) Limitations of low resolution mass spectrometry in the electron capture negative ionization mode for the analysis of short- and medium-chain chlorinated paraffins. Anal. Bioanal. Chem., 378, 1741-1747.
10. Coelhan, M., Saraci, M. and Parlar, H. (2000) A comparative study of polychlorinated alkanes as standards for the determination of C10-C13 polychlorinated paraffines in fish samples. Chemosphere, 40, 685-689.
11. Štejnarová, P., Coelhan, M., Kostrhounová, R., Parlar, H., and Holoubek, I. (2005) Analysis of short chain chlorinated paraffins in sediment samples from the Czech Republic by short-column GC/ECNI-MS. Chemosphere, 58, 253-262.
12. Lahaniatis, M.R., Coelhan, M. and Parlar, H. (2000) Clean-up and quantification of short and medium chain polychlorinated n-alkanes in fish, fish oil and fish feed. Organohalogen Compd., 47, 276-279.
13. Kosubová, P., Grabic, R. and Holoubek, I. (2005) Toxaphene and other chlorinated pesticides in the Czech mountain and lowland forest ecosystems. Fresen. Environ Bull., 14, 160-166.
14. Kosubová, P. (2004) Chirální environmentá lní polutanty - separace, stanovení, distribuce v prostředí. Doctoral thesis, RECETOX, Masaryk University, Faculty of Science, Brno, Czech Republic.
15. Kosubová, P., Grabic, R. and Holoubek, I. (2003) (HR)GC-MS/MS analysis of toxaphene congeners in various matrices from the Czech environent. Fresen. Environ. Bull., 12, 1303-1308.